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Assay Detail

CHEMBL5737706

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
IL-1 Secretion Assa: Monocytic THP-1 cells (ATCC: TIB-202) were maintained according to providers' instructions in RPMI media (RPMI/Hepes+10% fetal bovine serum+Sodium Pyruvate+0.05 mM Beta-mercaptoethanol (1000× stock)+Pen-Strep). Cells were differentiated in bulk with 0.5 μM phorbol 12-myristate 13-acetate (PMA; Sigma #P8139) for 3 hours, media was exchanged, and cells were plated at 50,000 cells per well in a 384-well flat-bottom cell culture plates (Greiner, #781986), and allowed to differentiate overnight. Compound in a 1:3.16 serial dilution series in DMSO was added 1:100 to the cells and incubated for 1 hour. The NLRP3 inflammasome was activated with the addition of 15 μM (final concentration) Nigericin (Enzo Life Sciences, #BML-CA421-0005), and cells were incubated for 3 hours. 10 μL supernatant was removed, and IL-1p levels were monitored using an HTRF assay (CisBio, #621L1PEC) according to manufacturers' instructions. Viability and pyroptosis was monitored with the addition of PrestoBlue cell viability reagent (Life Technologies, #A13261) directly to the cell culture plate.
351
Total Activities
114
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Interleukin-1 beta (CHEMBL1909490)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

NLRP3 inflammasome inhibitors
(2021)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 117 7.51 9.40
kon 117 - -
k_off 117 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5414596 3 9.40
CHEMBL5426651 3 9.40
CHEMBL5992744 3 9.22
CHEMBL5774519 3 9.15
CHEMBL5433380 3 9.10
CHEMBL5991941 3 9.10
CHEMBL5906571 3 9.10
CHEMBL5797061 3 9.10
CHEMBL5910216 3 9.10
CHEMBL5881090 3 9.05
CHEMBL6036597 3 8.92
CHEMBL5970809 3 8.89
CHEMBL5752218 6 8.89
CHEMBL5808276 3 8.80
CHEMBL5763108 3 8.80
CHEMBL5782617 6 8.74
CHEMBL5928082 3 8.72
CHEMBL5971979 3 8.72
CHEMBL6011033 3 8.64
CHEMBL6029082 3 8.59
CHEMBL5812129 3 8.59
CHEMBL5852308 6 8.52
CHEMBL5960754 3 8.52
CHEMBL5761984 3 8.49
CHEMBL5801636 3 8.49
CHEMBL6049792 3 8.48
CHEMBL6015148 3 8.46
CHEMBL5758980 3 8.44
CHEMBL6001622 3 8.33
CHEMBL5782662 3 8.23

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5414596 IC50 = 0.4 nM 9.40
CHEMBL5426651 IC50 = 0.4 nM 9.40
CHEMBL5992744 IC50 = 0.6 nM 9.22
CHEMBL5774519 IC50 = 0.7 nM 9.15
CHEMBL5797061 IC50 = 0.8 nM 9.10
CHEMBL5910216 IC50 = 0.8 nM 9.10
CHEMBL5433380 IC50 = 0.8 nM 9.10
CHEMBL5991941 IC50 = 0.8 nM 9.10
CHEMBL5906571 IC50 = 0.8 nM 9.10
CHEMBL5881090 IC50 = 0.9 nM 9.05
CHEMBL6036597 IC50 = 1.2 nM 8.92
CHEMBL5970809 IC50 = 1.3 nM 8.89
CHEMBL5752218 IC50 = 1.3 nM 8.89
CHEMBL5808276 IC50 = 1.6 nM 8.80
CHEMBL5763108 IC50 = 1.6 nM 8.80
CHEMBL5782617 IC50 = 1.8 nM 8.74
CHEMBL5971979 IC50 = 1.9 nM 8.72
CHEMBL5928082 IC50 = 1.9 nM 8.72
CHEMBL6011033 IC50 = 2.3 nM 8.64
CHEMBL6029082 IC50 = 2.6 nM 8.59
CHEMBL5812129 IC50 = 2.6 nM 8.59
CHEMBL5852308 IC50 = 3.0 nM 8.52
CHEMBL5960754 IC50 = 3.0 nM 8.52
CHEMBL5761984 IC50 = 3.2 nM 8.49
CHEMBL5801636 IC50 = 3.2 nM 8.49
CHEMBL6049792 IC50 = 3.3 nM 8.48
CHEMBL6015148 IC50 = 3.5 nM 8.46
CHEMBL5758980 IC50 = 3.6 nM 8.44
CHEMBL6001622 IC50 = 4.7 nM 8.33
CHEMBL5782662 IC50 = 5.9 nM 8.23
CHEMBL5840970 IC50 = 6.0 nM 8.22
CHEMBL5847930 IC50 = 6.3 nM 8.20
CHEMBL5973713 IC50 = 6.6 nM 8.18
CHEMBL5834410 IC50 = 6.8 nM 8.17
CHEMBL5963394 IC50 = 7.4 nM 8.13
CHEMBL5763742 IC50 = 7.6 nM 8.12
CHEMBL5882443 IC50 = 8.3 nM 8.08
CHEMBL5790303 IC50 = 10.2 nM 7.99
CHEMBL5984350 IC50 = 11.8 nM 7.93
CHEMBL5874946 IC50 = 13.0 nM 7.89
CHEMBL5808248 IC50 = 18.3 nM 7.74
CHEMBL5836561 IC50 = 22.7 nM 7.64
CHEMBL6015125 IC50 = 24.1 nM 7.62
CHEMBL6035509 IC50 = 25.3 nM 7.60
CHEMBL6009102 IC50 = 25.5 nM 7.59
CHEMBL5843429 IC50 = 26.0 nM 7.58
CHEMBL6023173 IC50 = 33.1 nM 7.48
CHEMBL5912010 IC50 = 35.9 nM 7.45
CHEMBL5745086 IC50 = 36.3 nM 7.44
CHEMBL5801025 IC50 = 40.1 nM 7.40