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Assay Detail

CHEMBL3705601

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Binding
Binding Assay: cDNA sequence encoding a mouse NPY Y5 receptor (Biochim. Biophys. Acta 1328:83-89, 1997) was cloned in a vector (pME18S, Takebe et al. Mol. Cell. Biol. 8, 8957). The obtained expression vector was transfected into CHO cells as a host by using Lipofect AMINE reagent (Trademark, Gico BRL Co., Ltd.) according to the instruction manual. The cells that stably express NPY Y5 receptor were obtained.The membranes prepared from the CHO cells expressing NPY Y5 receptor, the compound of this invention and 30,000 cpm [125I] peptide YY (60 pM of final concentration: Healthcare) were incubated in the assay buffer (20 mM HEPES-Hanks buffer containing 0.1% bovine serum albumin, pH 7.4) at 25° C. for 2 hours, and then the membrane was filtered from the mixture through a glass filter (GF/C) presoaked with 1% polyethyleneimine. After washing with 50 mM Tris-HCl buffer (pH 7.4), radioactivity retained on the filters was quantified with a gamma counter.
25
Total Activities
25
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Mus musculus
Cell Type CHO
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Neuropeptide Y receptor type 5 (CHEMBL3802)
Type SINGLE PROTEIN
Organism Mus musculus

Publication

5-membered ring heteroaromatic derivatives having NPY Y5 receptor antagonistic activity
(2014)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 25 9.16 9.89

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3666784 1 9.89
CHEMBL3666787 1 9.74
CHEMBL3666782 1 9.70
CHEMBL3666781 1 9.66
CHEMBL3666786 1 9.66
CHEMBL3666788 1 9.64
CHEMBL3666779 1 9.49
CHEMBL3666780 1 9.47
CHEMBL3666794 1 9.30
CHEMBL3666798 1 9.21
CHEMBL3666801 1 9.19
CHEMBL3666792 1 9.15
CHEMBL3666790 1 9.10
CHEMBL3666795 1 9.10
CHEMBL3666785 1 9.07
CHEMBL3666791 1 9.05
CHEMBL3666789 1 9.05
CHEMBL3666799 1 8.98
CHEMBL3666783 1 8.85
CHEMBL3666793 1 8.82
CHEMBL3666802 1 8.78
CHEMBL3666803 1 8.72
CHEMBL3666796 1 8.51
CHEMBL3666800 1 8.44
CHEMBL3666797 1 8.38

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3666784 IC50 = 0.13 nM 9.89
CHEMBL3666787 IC50 = 0.18 nM 9.74
CHEMBL3666782 IC50 = 0.2 nM 9.70
CHEMBL3666781 IC50 = 0.22 nM 9.66
CHEMBL3666786 IC50 = 0.22 nM 9.66
CHEMBL3666788 IC50 = 0.23 nM 9.64
CHEMBL3666779 IC50 = 0.32 nM 9.49
CHEMBL3666780 IC50 = 0.34 nM 9.47
CHEMBL3666794 IC50 = 0.5 nM 9.30
CHEMBL3666798 IC50 = 0.61 nM 9.21
CHEMBL3666801 IC50 = 0.65 nM 9.19
CHEMBL3666792 IC50 = 0.7 nM 9.15
CHEMBL3666790 IC50 = 0.8 nM 9.10
CHEMBL3666795 IC50 = 0.8 nM 9.10
CHEMBL3666785 IC50 = 0.86 nM 9.07
CHEMBL3666791 IC50 = 0.9 nM 9.05
CHEMBL3666789 IC50 = 0.9 nM 9.05
CHEMBL3666799 IC50 = 1.04 nM 8.98
CHEMBL3666783 IC50 = 1.4 nM 8.85
CHEMBL3666793 IC50 = 1.5 nM 8.82
CHEMBL3666802 IC50 = 1.67 nM 8.78
CHEMBL3666803 IC50 = 1.9 nM 8.72
CHEMBL3666796 IC50 = 3.1 nM 8.51
CHEMBL3666800 IC50 = 3.6 nM 8.44
CHEMBL3666797 IC50 = 4.21 nM 8.38