Skip to main content
Free research Free research Free assay review with research home and workspace preview
Quick search ChEMBL 36
Assay Detail

CHEMBL3705886

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition Assay: Reagents and consumables were purchased from Sigma Aldrich, Carna Biosciences, or Caliper Life Sciences. All assay reaction conditions for IC50 determinations were within the linear range with respect to time and enzyme concentration. In a 384 well polypropylene plate, c-FMS (0.14 nM, Carna 08-155) was pre-incubated in a 100 mM Hepes-NaOH pH 7.5 buffer containing 0.01% Triton X-100, 10 mM MgCl2, 0.1% BSA, 1 mM DTT, 10 uM sodium orthovanadate and 10 uM beta-glycerophosphate and compound with a concentration of 2.5% DMSO for 15 minutes at room temperature. The reaction was initiated with an equal volume of peptide substrate (Caliper Life Sciences catalog no. 760430) and ATP in the aforementioned buffer. The final concentrations in the reaction were 70 pM c-FMS, 1.5 uM peptide substrate and 500 uM ATP (ATP Km). The reaction was incubated at room temperature for 120 minutes and terminated with a buffer containing excess EDTA (100 mM Hepes-NaOH pH 7.5, 0.02% Brij, 0.1% CR-3.
80
Total Activities
79
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Macrophage colony-stimulating factor 1 receptor (CHEMBL1844)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Tropomyosin-related kinase (TRK) inhibitors
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 80 7.68 9.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3673440 1 9.00
CHEMBL3673486 1 8.70
CHEMBL3673438 1 8.70
CHEMBL3673442 1 8.70
CHEMBL3673436 1 8.70
CHEMBL3673462 1 8.70
CHEMBL3673453 1 8.70
CHEMBL3673452 GZ-389988 2.0 1 8.70
CHEMBL3673476 1 8.52
CHEMBL3673463 1 8.52
CHEMBL3673468 1 8.52
CHEMBL3673479 1 8.52
CHEMBL3673437 1 8.40
CHEMBL3673439 1 8.40
CHEMBL3673485 1 8.30
CHEMBL3673455 1 8.30
CHEMBL3678285 1 8.30
CHEMBL3673477 1 8.30
CHEMBL3673478 1 8.30
CHEMBL3673480 1 8.30
CHEMBL3673483 1 8.30
CHEMBL3673488 1 8.30
CHEMBL3673487 1 8.22
CHEMBL3673443 1 8.22
CHEMBL3673459 1 8.15
CHEMBL3678287 1 8.15
CHEMBL3673464 1 8.15
CHEMBL3673481 1 8.15
CHEMBL3673467 1 8.15
CHEMBL3678283 1 8.10

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3673440 IC50 = 1.0 nM 9.00
CHEMBL3673438 IC50 = 2.0 nM 8.70
CHEMBL3673486 IC50 = 2.0 nM 8.70
CHEMBL3673442 IC50 = 2.0 nM 8.70
CHEMBL3673436 IC50 = 2.0 nM 8.70
CHEMBL3673462 IC50 = 2.0 nM 8.70
CHEMBL3673453 IC50 = 2.0 nM 8.70
CHEMBL3673452 GZ-389988 IC50 = 2.0 nM 8.70
CHEMBL3673479 IC50 = 3.0 nM 8.52
CHEMBL3673476 IC50 = 3.0 nM 8.52
CHEMBL3673468 IC50 = 3.0 nM 8.52
CHEMBL3673463 IC50 = 3.0 nM 8.52
CHEMBL3673439 IC50 = 4.0 nM 8.40
CHEMBL3673437 IC50 = 4.0 nM 8.40
CHEMBL3673485 IC50 = 5.0 nM 8.30
CHEMBL3673483 IC50 = 5.0 nM 8.30
CHEMBL3673480 IC50 = 5.0 nM 8.30
CHEMBL3673478 IC50 = 5.0 nM 8.30
CHEMBL3673477 IC50 = 5.0 nM 8.30
CHEMBL3673455 IC50 = 5.0 nM 8.30
CHEMBL3678285 IC50 = 5.0 nM 8.30
CHEMBL3673488 IC50 = 5.0 nM 8.30
CHEMBL3673443 IC50 = 6.0 nM 8.22
CHEMBL3673487 IC50 = 6.0 nM 8.22
CHEMBL3673464 IC50 = 7.0 nM 8.15
CHEMBL3673459 IC50 = 7.0 nM 8.15
CHEMBL3673467 IC50 = 7.0 nM 8.15
CHEMBL3678287 IC50 = 7.0 nM 8.15
CHEMBL3673481 IC50 = 7.0 nM 8.15
CHEMBL3673456 IC50 = 8.0 nM 8.10
CHEMBL3678283 IC50 = 8.0 nM 8.10
CHEMBL3673482 IC50 = 9.0 nM 8.05
CHEMBL3678286 IC50 = 10.0 nM 8.00
CHEMBL3673484 IC50 = 11.0 nM 7.96
CHEMBL3673460 IC50 = 12.0 nM 7.92
CHEMBL3673448 IC50 = 12.0 nM 7.92
CHEMBL3673454 IC50 = 12.0 nM 7.92
CHEMBL3673466 IC50 = 13.0 nM 7.89
CHEMBL3673447 IC50 = 13.0 nM 7.89
CHEMBL3678289 IC50 = 13.0 nM 7.89
CHEMBL3673471 IC50 = 15.0 nM 7.82
CHEMBL3673465 IC50 = 15.0 nM 7.82
CHEMBL3673457 IC50 = 16.0 nM 7.80
CHEMBL3673454 IC50 = 16.0 nM 7.80
CHEMBL3678284 IC50 = 18.0 nM 7.75
CHEMBL3678297 IC50 = 19.0 nM 7.72
CHEMBL3678300 IC50 = 19.0 nM 7.72
CHEMBL3678302 IC50 = 25.0 nM 7.60
CHEMBL3673446 IC50 = 27.0 nM 7.57
CHEMBL3673489 IC50 = 28.0 nM 7.55