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Assay Detail

CHEMBL3705899

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
In Vitro Assay: Recombinant human factor D (expressed in E. coli and purified using standard methods) at 10 nM concentration is incubated with test compound at various concentrations for 1 hour at room temperature in 0.1 M Hepes buffer, pH 7.5, containing 1 mM MgCl2, 1 M NaCl and 0.05% CHAPS. A synthetic substrate Z-Lys-thiobenzyl and 2,4-dinitrobenzenesulfonyl-fluoresceine are added to final concentrations of 200 μM and 25 μM, respectively. The increase in fluorescence is recorded at excitation of 485 nm and emission at 535 nm in a microplate spectrofluorimeter. IC50 values are calculated from percentage of inhibition of complement factor D-activity as a function of test compound concentration.
773
Total Activities
768
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Complement factor D (CHEMBL2176771)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Complement pathway modulators and uses thereof
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 773 6.81 9.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL2180765 1 9.00
CHEMBL2180764 1 8.70
CHEMBL3678905 1 8.52
CHEMBL3683717 2 8.52
CHEMBL3678945 1 8.52
CHEMBL3678910 1 8.52
CHEMBL3673804 1 8.52
CHEMBL3673802 1 8.52
CHEMBL3673750 1 8.52
CHEMBL3673724 1 8.52
CHEMBL3668673 1 8.52
CHEMBL2180766 1 8.52
CHEMBL3673812 1 8.40
CHEMBL3683739 1 8.40
CHEMBL3683725 1 8.40
CHEMBL3683724 1 8.40
CHEMBL3683720 1 8.40
CHEMBL3678944 1 8.40
CHEMBL3673738 1 8.40
CHEMBL3673732 1 8.40
CHEMBL3668636 1 8.40
CHEMBL3668669 1 8.30
CHEMBL3673726 1 8.30
CHEMBL3673793 1 8.30
CHEMBL3673808 1 8.30
CHEMBL3678852 1 8.30
CHEMBL3678898 1 8.30
CHEMBL3683719 1 8.30
CHEMBL3965664 1 8.30
CHEMBL3683730 1 8.30

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL2180765 IC50 = 1.0 nM 9.00
CHEMBL2180764 IC50 = 2.0 nM 8.70
CHEMBL3683717 IC50 = 3.0 nM 8.52
CHEMBL3678945 IC50 = 3.0 nM 8.52
CHEMBL2180766 IC50 = 3.0 nM 8.52
CHEMBL3673724 IC50 = 3.0 nM 8.52
CHEMBL3668673 IC50 = 3.0 nM 8.52
CHEMBL3678910 IC50 = 3.0 nM 8.52
CHEMBL3673750 IC50 = 3.0 nM 8.52
CHEMBL3678905 IC50 = 3.0 nM 8.52
CHEMBL3673802 IC50 = 3.0 nM 8.52
CHEMBL3673804 IC50 = 3.0 nM 8.52
CHEMBL3683739 IC50 = 4.0 nM 8.40
CHEMBL3683720 IC50 = 4.0 nM 8.40
CHEMBL3678944 IC50 = 4.0 nM 8.40
CHEMBL3673732 IC50 = 4.0 nM 8.40
CHEMBL3683724 IC50 = 4.0 nM 8.40
CHEMBL3683725 IC50 = 4.0 nM 8.40
CHEMBL3673738 IC50 = 4.0 nM 8.40
CHEMBL3668636 IC50 = 4.0 nM 8.40
CHEMBL3673812 IC50 = 4.0 nM 8.40
CHEMBL3678898 IC50 = 5.0 nM 8.30
CHEMBL3683730 IC50 = 5.0 nM 8.30
CHEMBL3683737 IC50 = 5.0 nM 8.30
CHEMBL3965664 IC50 = 5.0 nM 8.30
CHEMBL3683719 IC50 = 5.0 nM 8.30
CHEMBL3683717 IC50 = 5.0 nM 8.30
CHEMBL3668669 IC50 = 5.0 nM 8.30
CHEMBL3673793 IC50 = 5.0 nM 8.30
CHEMBL3673808 IC50 = 5.0 nM 8.30
CHEMBL3678852 IC50 = 5.0 nM 8.30
CHEMBL3673726 IC50 = 5.0 nM 8.30
CHEMBL3678879 IC50 = 6.0 nM 8.22
CHEMBL3678913 IC50 = 6.0 nM 8.22
CHEMBL3678906 IC50 = 6.0 nM 8.22
CHEMBL3668685 IC50 = 6.0 nM 8.22
CHEMBL3668710 IC50 = 6.0 nM 8.22
CHEMBL3668640 IC50 = 6.0 nM 8.22
CHEMBL3683722 IC50 = 7.0 nM 8.15
CHEMBL3673730 IC50 = 7.0 nM 8.15
CHEMBL3663978 IC50 = 7.0 nM 8.15
CHEMBL3683732 IC50 = 7.0 nM 8.15
CHEMBL3663968 IC50 = 7.0 nM 8.15
CHEMBL3683746 IC50 = 7.0 nM 8.15
CHEMBL3673860 IC50 = 7.0 nM 8.15
CHEMBL3673821 IC50 = 7.0 nM 8.15
CHEMBL3673814 IC50 = 7.0 nM 8.15
CHEMBL3673752 IC50 = 7.0 nM 8.15
CHEMBL3673822 IC50 = 7.0 nM 8.15
CHEMBL3668711 IC50 = 7.0 nM 8.15