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Assay Detail

CHEMBL3706188

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibitory Assay: This test is based on measuring the expression of the AKT protein phosphorylated on serine 473. The phosphorylation of AKT (pAKT) is measured by western blotting in the PC3 human prostate carcinoma line (ATCC CRL-1435), using an antibody that specifically recognises pAKT-S473.On day 1, the PC3 cells are seeded into 6-well plates (TPP, #92006) at the concentration of 0.8x106 cells/well in 1800 ul of DMEM medium (DMEM Gibco #11960-044) containing 10% of foetal calf serum (SVF Gibco, #10500-056) and 1% glutamine (L-Glu Gibco #25030-024), and incubated at 37 C., 5% CO2, overnight.On day 2, the cells are incubated in the presence or absence of the test products for 1 to 2 hours at 37 C. in the presence of 5% CO2. The molecules, diluted in dimethyl sulphoxide (DMSO Sigma #D2650), are added from a 10-times concentrated stock solution, the final percentage of DMSO being 0.1%. The molecules are tested either at a single concentration of less than or equal to 10 uM, or ....
55
Total Activities
55
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type PC-3
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

RAC-alpha serine/threonine-protein kinase (CHEMBL4282)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

(6-oxo-1,6-dihydropyrimidin-2-yl)amide derivatives, preparation thereof and pharmaceutical use thereof as AKT(PKB) phosphorylation inhibitors
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 55 6.18 7.64

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL2151923 1 7.64
CHEMBL2151924 1 7.64
CHEMBL2151919 1 7.41
CHEMBL2151048 1 7.03
CHEMBL2151921 1 7.00
CHEMBL3696234 1 6.99
CHEMBL2151926 1 6.94
CHEMBL3112690 1 6.88
CHEMBL3696272 1 6.86
CHEMBL2151925 1 6.77
CHEMBL3696265 1 6.74
CHEMBL2151935 1 6.70
CHEMBL3696253 1 6.70
CHEMBL3696268 1 6.64
CHEMBL3696282 1 6.60
CHEMBL3696262 1 6.58
CHEMBL3696258 1 6.54
CHEMBL3696261 1 6.51
CHEMBL2151927 1 6.50
CHEMBL2151821 1 6.49
CHEMBL3696244 1 6.46
CHEMBL3696264 1 6.46
CHEMBL3696259 1 6.40
CHEMBL3696274 1 6.38
CHEMBL3696255 1 6.32
CHEMBL3696277 1 6.28
CHEMBL3696260 1 6.26
CHEMBL2151820 1 6.24
CHEMBL3696251 1 6.21
CHEMBL3696238 1 6.20

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL2151923 IC50 = 23.0 nM 7.64
CHEMBL2151924 IC50 = 23.0 nM 7.64
CHEMBL2151919 IC50 = 39.0 nM 7.41
CHEMBL2151048 IC50 = 93.0 nM 7.03
CHEMBL2151921 IC50 = 100.0 nM 7.00
CHEMBL3696234 IC50 = 102.0 nM 6.99
CHEMBL2151926 IC50 = 116.0 nM 6.94
CHEMBL3112690 IC50 = 133.0 nM 6.88
CHEMBL3696272 IC50 = 137.0 nM 6.86
CHEMBL2151925 IC50 = 171.0 nM 6.77
CHEMBL3696265 IC50 = 184.0 nM 6.74
CHEMBL2151935 IC50 = 202.0 nM 6.70
CHEMBL3696253 IC50 = 200.0 nM 6.70
CHEMBL3696268 IC50 = 227.0 nM 6.64
CHEMBL3696282 IC50 = 250.0 nM 6.60
CHEMBL3696262 IC50 = 261.0 nM 6.58
CHEMBL3696258 IC50 = 290.0 nM 6.54
CHEMBL3696261 IC50 = 308.0 nM 6.51
CHEMBL2151927 IC50 = 318.0 nM 6.50
CHEMBL2151821 IC50 = 321.0 nM 6.49
CHEMBL3696244 IC50 = 350.0 nM 6.46
CHEMBL3696264 IC50 = 346.0 nM 6.46
CHEMBL3696259 IC50 = 400.0 nM 6.40
CHEMBL3696274 IC50 = 417.0 nM 6.38
CHEMBL3696255 IC50 = 480.0 nM 6.32
CHEMBL3696277 IC50 = 530.0 nM 6.28
CHEMBL3696260 IC50 = 549.0 nM 6.26
CHEMBL2151820 IC50 = 570.0 nM 6.24
CHEMBL3696251 IC50 = 609.0 nM 6.21
CHEMBL3696238 IC50 = 632.0 nM 6.20
CHEMBL3696286 IC50 = 650.0 nM 6.19
CHEMBL2151819 IC50 = 727.0 nM 6.14
CHEMBL3639951 IC50 = 737.0 nM 6.13
CHEMBL3696273 IC50 = 760.0 nM 6.12
CHEMBL3696270 IC50 = 807.0 nM 6.09
CHEMBL2151922 IC50 = 850.0 nM 6.07
CHEMBL3696242 IC50 = 1314.0 nM 5.88
CHEMBL2151920 IC50 = 1420.0 nM 5.85
CHEMBL3696240 IC50 = 1481.0 nM 5.83
CHEMBL3696257 IC50 = 1494.0 nM 5.83
CHEMBL3696256 IC50 = 1763.0 nM 5.75
CHEMBL3696281 IC50 = 2207.0 nM 5.66
CHEMBL3696246 IC50 = 2287.0 nM 5.64
CHEMBL3696263 IC50 = 2498.0 nM 5.60
CHEMBL2151822 IC50 = 3498.0 nM 5.46
CHEMBL3696250 IC50 = 3635.0 nM 5.44
CHEMBL3696284 IC50 = 5375.0 nM 5.27
CHEMBL2151928 IC50 = 5865.0 nM 5.23
CHEMBL2151929 IC50 = 6155.0 nM 5.21
CHEMBL3696279 IC50 = 6460.0 nM 5.19