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Assay Detail

CHEMBL3706312

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Kinase Glo Assay: Human RSK2 protein, purchased from Invitrogen, is used to measure kinase activity utilizing Kinase Glo Plus (Promega) a homogeneous assay technology, which uses a luciferin-luciferase based ATP detection reagent to quantify residual ATP. The assay is performed using 0.75 nM His-RSK2, 0.75 uM ATP and 1.0 uM S6 Kinase/RSK Substrate Peptide 1 (Upstate, catalog #12-124), in assay buffer consisting of 25 mM HEPES, pH 7.5, 10 mM MgCl2, 5 mM MnCl2, 50 mM KCl, 0.2% BSA, 0.01% CHAPS, 100 uM Na3VO4, 0.5 mM DTT, and 1% DMSO. Solutions of test compounds at various concentrations are prepared by 1:3 fold serial dilution of a 1 mM solution of compound in DMSO. The DMSO solutions are further diluted with assay buffer to a final concentration of DMSO of 5%.The assay is performed in a 384 well, white, non-binding plate (Corning, catalogue #3574). Solutions of test compounds (10 uL) are transferred to a dry assay plate, followed by addition of 20 uL kinase.
105
Total Activities
105
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Ribosomal protein S6 kinase alpha-3 (CHEMBL2345)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Heterocyclic compounds containing a pyrrolopyridine or benzimidazole core
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 105 7.39 9.70

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3673622 1 9.70
CHEMBL3673631 1 9.57
CHEMBL3673624 1 9.47
CHEMBL3673609 1 9.41
CHEMBL3673603 1 9.11
CHEMBL3673606 1 8.96
CHEMBL3673598 1 8.80
CHEMBL3639725 1 8.80
CHEMBL3673592 1 8.68
CHEMBL3673589 1 8.64
CHEMBL3673595 1 8.64
CHEMBL3673648 1 8.59
CHEMBL3673625 1 8.52
CHEMBL3673627 1 8.52
CHEMBL3673657 1 8.48
CHEMBL3673658 1 8.44
CHEMBL3673601 1 8.42
CHEMBL3673610 1 8.42
CHEMBL3673661 1 8.41
CHEMBL3673629 1 8.40
CHEMBL3673644 1 8.37
CHEMBL3673581 1 8.33
CHEMBL3673604 1 8.32
CHEMBL3673662 1 8.29
CHEMBL3673645 1 8.28
CHEMBL3673567 1 8.26
CHEMBL3673630 1 8.21
CHEMBL3673647 1 8.18
CHEMBL3673612 1 8.17
CHEMBL3673586 1 8.04

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3673622 IC50 = 0.2 nM 9.70
CHEMBL3673631 IC50 = 0.27 nM 9.57
CHEMBL3673624 IC50 = 0.34 nM 9.47
CHEMBL3673609 IC50 = 0.39 nM 9.41
CHEMBL3673603 IC50 = 0.78 nM 9.11
CHEMBL3673606 IC50 = 1.1 nM 8.96
CHEMBL3639725 IC50 = 1.6 nM 8.80
CHEMBL3673598 IC50 = 1.6 nM 8.80
CHEMBL3673592 IC50 = 2.1 nM 8.68
CHEMBL3673589 IC50 = 2.3 nM 8.64
CHEMBL3673595 IC50 = 2.3 nM 8.64
CHEMBL3673648 IC50 = 2.6 nM 8.59
CHEMBL3673625 IC50 = 3.0 nM 8.52
CHEMBL3673627 IC50 = 3.0 nM 8.52
CHEMBL3673657 IC50 = 3.3 nM 8.48
CHEMBL3673658 IC50 = 3.6 nM 8.44
CHEMBL3673610 IC50 = 3.8 nM 8.42
CHEMBL3673601 IC50 = 3.8 nM 8.42
CHEMBL3673661 IC50 = 3.9 nM 8.41
CHEMBL3673629 IC50 = 4.0 nM 8.40
CHEMBL3673644 IC50 = 4.3 nM 8.37
CHEMBL3673581 IC50 = 4.7 nM 8.33
CHEMBL3673604 IC50 = 4.8 nM 8.32
CHEMBL3673662 IC50 = 5.1 nM 8.29
CHEMBL3673645 IC50 = 5.2 nM 8.28
CHEMBL3673567 IC50 = 5.5 nM 8.26
CHEMBL3673630 IC50 = 6.1 nM 8.21
CHEMBL3673647 IC50 = 6.6 nM 8.18
CHEMBL3673612 IC50 = 6.7 nM 8.17
CHEMBL3673586 IC50 = 9.2 nM 8.04
CHEMBL3673607 IC50 = 9.7 nM 8.01
CHEMBL3673636 IC50 = 11.6 nM 7.94
CHEMBL3673623 IC50 = 12.0 nM 7.92
CHEMBL3673611 IC50 = 12.0 nM 7.92
CHEMBL3673659 IC50 = 13.0 nM 7.89
CHEMBL3673599 IC50 = 13.0 nM 7.89
CHEMBL3673632 IC50 = 15.0 nM 7.82
CHEMBL3673667 IC50 = 17.0 nM 7.77
CHEMBL3673642 IC50 = 19.0 nM 7.72
CHEMBL3673643 IC50 = 19.0 nM 7.72
CHEMBL3673588 IC50 = 20.0 nM 7.70
CHEMBL3673596 IC50 = 20.0 nM 7.70
CHEMBL3673580 IC50 = 23.0 nM 7.64
CHEMBL3673600 IC50 = 25.0 nM 7.60
CHEMBL3673593 IC50 = 25.0 nM 7.60
CHEMBL3673635 IC50 = 26.5 nM 7.58
CHEMBL3673633 IC50 = 27.0 nM 7.57
CHEMBL3673640 IC50 = 29.0 nM 7.54
CHEMBL3639724 IC50 = 33.0 nM 7.48
CHEMBL3673628 IC50 = 34.0 nM 7.47