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Assay Detail

CHEMBL3707790

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
FLIPR Assay: 1321N1 cells expressing the recombinant human, rat or mouse P2X7 channel was cultured in HyQ DME/(HyClone/Dulbecco's Modified Eagle Medium) high glucose supplemented with 10% Fetal Bovine Serum (FBS) and appropriate selection marker. Cells were seeded at a density of 25000 cells/well (96-well clear bottom black walled plates) in 100 ul volume/well. On the day of the experiment, cell plates were washed with assay buffer, containing (in mM): 130 NaCl, 2 KCl, 1 CaCl2, 1 MgCl2, 10 HEPES, 5 glucose; pH 7.40 and 300 mOs. After the wash, cells were loaded with the Calcium-4 dye (Molecular Device) and incubated in the dark for 60 minutes. Test compounds were prepared at 250x the test concentration in neat DMSO. Intermediate 96-well compound plates were prepared by transferring 1.2 uL of the compound into 300 uL of assay buffer. A further 3x dilution occurred when transferring 50 uL/well of the compound plate to 100 uL/well in the cell plate.
112
Total Activities
110
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Cell Type 1321-N1
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

P2X purinoceptor 7 (CHEMBL2496)
Type SINGLE PROTEIN
Organism Rattus norvegicus

Publication

P2X7 modulators
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 112 6.67 8.62

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3674090 1 8.62
CHEMBL3674082 1 8.60
CHEMBL3674081 1 8.25
CHEMBL3674094 1 8.11
CHEMBL3674070 1 8.10
CHEMBL3674129 1 8.07
CHEMBL3674087 1 8.06
CHEMBL3674126 1 8.04
CHEMBL3674139 1 8.01
CHEMBL3674093 1 8.00
CHEMBL3674051 1 8.00
CHEMBL3674085 1 8.00
CHEMBL3674077 1 7.99
CHEMBL3674075 1 7.91
CHEMBL3674089 1 7.91
CHEMBL3674116 1 7.90
CHEMBL3674097 1 7.89
CHEMBL3674137 1 7.89
CHEMBL3674119 1 7.89
CHEMBL3674083 1 7.88
CHEMBL3674103 1 7.88
CHEMBL3674128 1 7.85
CHEMBL3674086 1 7.84
CHEMBL3674115 1 7.83
CHEMBL3674102 1 7.83
CHEMBL3674105 1 7.82
CHEMBL3674100 1 7.82
CHEMBL3674125 1 7.80
CHEMBL3674107 1 7.80
CHEMBL3674092 1 7.75

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3674090 IC50 = 2.4 nM 8.62
CHEMBL3674082 IC50 = 2.5 nM 8.60
CHEMBL3674081 IC50 = 5.6 nM 8.25
CHEMBL3674094 IC50 = 7.7 nM 8.11
CHEMBL3674070 IC50 = 7.9 nM 8.10
CHEMBL3674129 IC50 = 8.6 nM 8.07
CHEMBL3674087 IC50 = 8.8 nM 8.06
CHEMBL3674126 IC50 = 9.1 nM 8.04
CHEMBL3674139 IC50 = 9.7 nM 8.01
CHEMBL3674085 IC50 = 10.0 nM 8.00
CHEMBL3674093 IC50 = 10.0 nM 8.00
CHEMBL3674051 IC50 = 9.9 nM 8.00
CHEMBL3674077 IC50 = 10.3 nM 7.99
CHEMBL3674075 IC50 = 12.4 nM 7.91
CHEMBL3674089 IC50 = 12.4 nM 7.91
CHEMBL3674116 IC50 = 12.6 nM 7.90
CHEMBL3674119 IC50 = 13.0 nM 7.89
CHEMBL3674137 IC50 = 12.9 nM 7.89
CHEMBL3674097 IC50 = 12.9 nM 7.89
CHEMBL3674103 IC50 = 13.1 nM 7.88
CHEMBL3674083 IC50 = 13.3 nM 7.88
CHEMBL3674128 IC50 = 14.2 nM 7.85
CHEMBL3674086 IC50 = 14.5 nM 7.84
CHEMBL3674115 IC50 = 14.9 nM 7.83
CHEMBL3674102 IC50 = 14.9 nM 7.83
CHEMBL3674100 IC50 = 15.3 nM 7.82
CHEMBL3674105 IC50 = 15.2 nM 7.82
CHEMBL3674125 IC50 = 16.0 nM 7.80
CHEMBL3674107 IC50 = 15.9 nM 7.80
CHEMBL3674092 IC50 = 17.8 nM 7.75
CHEMBL3674099 IC50 = 20.0 nM 7.70
CHEMBL3674096 IC50 = 20.0 nM 7.70
CHEMBL3674131 IC50 = 21.0 nM 7.68
CHEMBL3674118 IC50 = 23.0 nM 7.64
CHEMBL3674121 IC50 = 23.7 nM 7.62
CHEMBL3674066 IC50 = 25.1 nM 7.60
CHEMBL3674132 IC50 = 28.4 nM 7.55
CHEMBL3674056 IC50 = 67.9 nM 7.17
CHEMBL3674056 IC50 = 67.9 nM 7.17
CHEMBL3674050 IC50 = 76.2 nM 7.12
CHEMBL3674112 IC50 = 101.4 nM 6.99
CHEMBL3674074 IC50 = 117.2 nM 6.93
CHEMBL3674095 IC50 = 126.2 nM 6.90
CHEMBL3674134 IC50 = 127.9 nM 6.89
CHEMBL3674135 IC50 = 127.9 nM 6.89
CHEMBL3674108 IC50 = 131.8 nM 6.88
CHEMBL3674069 IC50 = 156.0 nM 6.81
CHEMBL3674068 IC50 = 158.5 nM 6.80
CHEMBL3674076 IC50 = 161.1 nM 6.79
CHEMBL3674127 IC50 = 166.0 nM 6.78