Skip to main content
Free research Free research Free assay review with research home and workspace preview
Quick search ChEMBL 36
Assay Detail

CHEMBL3707863

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
FLIPR Assay: Ca2+ Flux: 1321N1 cells expressing the recombinant human, rat or mouse P2X7 channel was cultured in HyQ DME/(HyClone/Dulbecco's Modified Eagle Medium) high glucose supplemented with 10% Fetal Bovine Serum (FBS) and appropriate selection marker. Cells were seeded at a density of 25000 cells/well (96-well clear bottom black walled plates) in 100 ul volume/well. On the day of the experiment, cell plates were washed with assay buffer, containing (in mM): 130 NaCl, 2 KCl, 1 CaCl2, 1 MgCl2, 10 HEPES, 5 glucose; pH 7.40 and 300 mOs. After the wash, cells were loaded with the Calcium-4 dye (Molecular Device) and incubated in the dark for 60 minutes. Test compounds were prepared at 250x the test concentration in neat DMSO. Intermediate 96-well compound plates were prepared by transferring 1.2 uL of the compound into 300 uL of assay buffer. A further 3x dilution occurred when transferring 50 uL/well of the compound plate to 100 uL/well in the cell plate.
92
Total Activities
90
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Cell Type 1321-N1
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

P2X purinoceptor 7 (CHEMBL2496)
Type SINGLE PROTEIN
Organism Rattus norvegicus

Publication

[1,2,4]triazolo[4,3-a]pyrazines as P2X7 modulators
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 92 6.20 8.34

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3663287 1 8.34
CHEMBL3663296 1 8.29
CHEMBL3663316 2 8.25
CHEMBL3663294 2 8.25
CHEMBL3663253 1 8.16
CHEMBL3663289 1 8.09
CHEMBL3663286 1 8.02
CHEMBL3663260 1 7.97
CHEMBL3663291 1 7.93
CHEMBL3663257 1 7.80
CHEMBL3663284 1 7.80
CHEMBL3663277 1 7.75
CHEMBL3663240 1 7.30
CHEMBL3663242 1 7.19
CHEMBL3663239 1 6.99
CHEMBL3663254 1 6.91
CHEMBL3663297 1 6.90
CHEMBL3663295 1 6.88
CHEMBL3663256 1 6.87
CHEMBL3663270 1 6.81
CHEMBL3663298 1 6.80
CHEMBL3663259 1 6.76
CHEMBL3663255 1 6.73
CHEMBL3663290 1 6.55
CHEMBL3663237 1 6.52
CHEMBL3663244 1 6.50
CHEMBL3663252 1 6.43
CHEMBL3663288 1 6.40
CHEMBL3663292 1 6.40
CHEMBL3639621 1 6.26

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3663287 IC50 = 4.6 nM 8.34
CHEMBL3663296 IC50 = 5.1 nM 8.29
CHEMBL3663316 IC50 = 5.6 nM 8.25
CHEMBL3663294 IC50 = 5.6 nM 8.25
CHEMBL3663253 IC50 = 6.9 nM 8.16
CHEMBL3663289 IC50 = 8.2 nM 8.09
CHEMBL3663286 IC50 = 9.6 nM 8.02
CHEMBL3663294 IC50 = 10.3 nM 7.99
CHEMBL3663260 IC50 = 10.6 nM 7.97
CHEMBL3663291 IC50 = 11.8 nM 7.93
CHEMBL3663257 IC50 = 16.0 nM 7.80
CHEMBL3663284 IC50 = 16.0 nM 7.80
CHEMBL3663277 IC50 = 17.6 nM 7.75
CHEMBL3663316 IC50 = 36.1 nM 7.44
CHEMBL3663240 IC50 = 49.5 nM 7.30
CHEMBL3663242 IC50 = 64.6 nM 7.19
CHEMBL3663239 IC50 = 102.6 nM 6.99
CHEMBL3663254 IC50 = 122.2 nM 6.91
CHEMBL3663297 IC50 = 125.9 nM 6.90
CHEMBL3663295 IC50 = 132.7 nM 6.88
CHEMBL3663256 IC50 = 134.6 nM 6.87
CHEMBL3663270 IC50 = 154.5 nM 6.81
CHEMBL3663298 IC50 = 158.5 nM 6.80
CHEMBL3663259 IC50 = 174.6 nM 6.76
CHEMBL3663255 IC50 = 187.9 nM 6.73
CHEMBL3663290 IC50 = 282.5 nM 6.55
CHEMBL3663237 IC50 = 300.6 nM 6.52
CHEMBL3663244 IC50 = 316.2 nM 6.50
CHEMBL3663252 IC50 = 375.0 nM 6.43
CHEMBL3663288 IC50 = 396.3 nM 6.40
CHEMBL3663292 IC50 = 398.1 nM 6.40
CHEMBL3639621 IC50 = 543.3 nM 6.26
CHEMBL3663305 IC50 = 707.9 nM 6.15
CHEMBL3663278 IC50 = 743.0 nM 6.13
CHEMBL3663293 IC50 = 794.3 nM 6.10
CHEMBL3663279 IC50 = 824.1 nM 6.08
CHEMBL3663261 IC50 = 1064.1 nM 5.97
CHEMBL3663282 IC50 = 1142.9 nM 5.94
CHEMBL3663262 IC50 = 1213.4 nM 5.92
CHEMBL3663249 IC50 = 1220.4 nM 5.91
CHEMBL3663265 IC50 = 1303.2 nM 5.88
CHEMBL3663306 IC50 = 1370.9 nM 5.86
CHEMBL3663307 IC50 = 1556.0 nM 5.81
CHEMBL3663247 IC50 = 1584.9 nM 5.80
CHEMBL3663243 IC50 = 1650.1 nM 5.78
CHEMBL3663246 IC50 = 1995.3 nM 5.70
CHEMBL3663232 IC50 = 2564.5 nM 5.59
CHEMBL3663263 IC50 = 2606.2 nM 5.58
CHEMBL3663266 IC50 = 2779.7 nM 5.56
CHEMBL3663313 IC50 = 3047.9 nM 5.52