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Assay Detail

CHEMBL3707872

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Luciferase-Based Assay: Recombinant human c-Src or Yes (28 ng/well, Panvera/Invitrogen, Madison Wis.), ATP (3 μM), a tyrosine kinase substrate (PTK2, 250 μM, Promega Corp., Madison Wis.), and test agents (at concentrations ranging from about 1 nM/l to about 100 μM/l), in the presence of Src kinase reaction buffer (Upstate USA, Lake Placid N.Y.). After reacting for about 90 minutes at room temperature, residual ATP was determined using a luciferase-based assay (KinaseGlo, Promega Corp.) as a measure of kinase activity.
16
Total Activities
16
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Tyrosine-protein kinase Yes (CHEMBL2073)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Benzotriazine inhibitors of kinases
(2013)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 16 8.11 9.30

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL400402 1 9.30
CHEMBL3651257 1 9.15
CHEMBL3651296 1 8.92
CHEMBL3651228 1 8.91
CHEMBL249821 1 8.89
CHEMBL3651297 1 8.59
CHEMBL231218 1 8.51
CHEMBL218549 1 8.43
CHEMBL3648061 1 8.14
CHEMBL230614 1 8.11
CHEMBL230686 1 7.99
CHEMBL3648058 1 7.74
CHEMBL268825 1 7.66
CHEMBL230685 1 6.96
CHEMBL3651299 1 6.33
CHEMBL218042 1 6.08

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL400402 IC50 = 0.5 nM 9.30
CHEMBL3651257 IC50 = 0.7 nM 9.15
CHEMBL3651296 IC50 = 1.2 nM 8.92
CHEMBL3651228 IC50 = 1.24 nM 8.91
CHEMBL249821 IC50 = 1.28 nM 8.89
CHEMBL3651297 IC50 = 2.6 nM 8.59
CHEMBL231218 IC50 = 3.1 nM 8.51
CHEMBL218549 IC50 = 3.7 nM 8.43
CHEMBL3648061 IC50 = 7.3 nM 8.14
CHEMBL230614 IC50 = 7.7 nM 8.11
CHEMBL230686 IC50 = 10.3 nM 7.99
CHEMBL3648058 IC50 = 18.3 nM 7.74
CHEMBL268825 IC50 = 21.7 nM 7.66
CHEMBL230685 IC50 = 111.0 nM 6.96
CHEMBL3651299 IC50 = 465.0 nM 6.33
CHEMBL218042 IC50 = 822.0 nM 6.08