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Assay Detail

CHEMBL3887185

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition Assay: The object of this assay was to test the inventive compounds for the kinase inhibitory activity in vitro. In this assay, an isotopic labeling method was used to label the gamma phosphate group on ATP. EGFR (including wild type, L858R mutant type and L858R/T790M double mutant type), VEGFR2, ALK, BTK, c-KIT, c-SRC, MET, PDGFRalpha and FLT3 kinases were tested in vitro for the activity inhibition. Staurosporine was used as a reference molecule (or referred to as a positive control). The kinase inhibitory activities of the tested compounds were expressed in the IC50 value (half inhibition concentration) or the kinase activity inhibitory rate by the tested compounds at 10 uM. The IC50 value can be obtained by the calculation of the inhibitory rates at a series of different concentrations of the tested compounds. 1. Materials: 20mM 3-(N-morpholinyl)propylsulfonic acid (MOPS); 1mM Ethylenediaminetetraacetic acid (EDTA); 0.01% Polyethylene glycol lauryl ether (Brij-35).
27
Total Activities
26
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Epidermal growth factor receptor (CHEMBL203)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Arylamino purine derivatives, preparation method and pharmaceutical use thereof
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 27 8.53 9.40

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3678946 1 9.40
CHEMBL3674150 2 9.40
CHEMBL3678960 1 9.22
CHEMBL3678952 1 9.00
CHEMBL3678951 1 9.00
CHEMBL3678950 1 9.00
CHEMBL3674148 1 9.00
CHEMBL3674152 1 9.00
CHEMBL2178350 1 8.70
CHEMBL3678948 1 8.52
CHEMBL3678949 1 8.52
CHEMBL2178349 1 8.52
CHEMBL3678958 RUSERONTINIB 3.0 1 8.40
CHEMBL3678954 1 8.40
CHEMBL3678947 1 8.40
CHEMBL3678955 1 8.30
CHEMBL3678959 1 8.30
CHEMBL3678957 1 8.30
CHEMBL2178368 1 8.30
CHEMBL3678953 1 8.30
CHEMBL3674151 1 8.30
CHEMBL2178351 1 8.30
CHEMBL4113919 1 8.10
CHEMBL3678956 1 8.00
CHEMBL4111809 1 7.22
CHEMBL2178352 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3674150 IC50 = 0.4 nM 9.40
CHEMBL3678946 IC50 = 0.4 nM 9.40
CHEMBL3678960 IC50 = 0.6 nM 9.22
CHEMBL3678951 IC50 = 1.0 nM 9.00
CHEMBL3678952 IC50 = 1.0 nM 9.00
CHEMBL3678950 IC50 = 1.0 nM 9.00
CHEMBL3674148 IC50 = 1.0 nM 9.00
CHEMBL3674152 IC50 = 1.0 nM 9.00
CHEMBL2178350 IC50 = 2.0 nM 8.70
CHEMBL2178349 IC50 = 3.0 nM 8.52
CHEMBL3678948 IC50 = 3.0 nM 8.52
CHEMBL3678949 IC50 = 3.0 nM 8.52
CHEMBL3678958 RUSERONTINIB IC50 = 4.0 nM 8.40
CHEMBL3678947 IC50 = 4.0 nM 8.40
CHEMBL3678954 IC50 = 4.0 nM 8.40
CHEMBL3678953 IC50 = 5.0 nM 8.30
CHEMBL3678955 IC50 = 5.0 nM 8.30
CHEMBL2178368 IC50 = 5.0 nM 8.30
CHEMBL3678957 IC50 = 5.0 nM 8.30
CHEMBL2178351 IC50 = 5.0 nM 8.30
CHEMBL3678959 IC50 = 5.0 nM 8.30
CHEMBL3674151 IC50 = 5.0 nM 8.30
CHEMBL4113919 IC50 = 8.0 nM 8.10
CHEMBL3678956 IC50 = 10.0 nM 8.00
CHEMBL3674150 IC50 = 18.0 nM 7.75
CHEMBL4111809 IC50 = 60.0 nM 7.22
CHEMBL2178352 IC50 = 0.4 nM -