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Assay Detail

CHEMBL3887482

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Functional
cAMP Assay: 1. Seed cells on an EP2 or EP4 STEP plate at a density of 40,000-80,000 cells/well in 200 uL of reduced serum medium containing 0.5% FBS. Place the plate in a 37° C. incubator with 5% CO2 and incubate overnight. 2. After 16-18 hours of incubation, aspirate the culture media from each well. 3. Add 200 ul of culture medium containing 500 uM IBMX (an inhibitor of cAMP phosphodiesterase) and different concentration of test compounds to the assigned wells. For each test compound, at least 8 concentrations starting at highest 10 M and lowest 0.01 pM were tested. In addition each concentration had triplicates. A PGE2 curve (concentrations from lowest to highest, 0 pM, 0.384 pM, 1.92 pM, 9.6 pM, 48 pM, 240 pM, 1200 pM, and 6000 pM) was always run in parallel with test compounds. 4. Incubate the cells in a cell culture incubator for 30 minutes. 5. Centrifuge the plate at 1,000x rpm for 10 minutes. 6. Aspirate the supernatant.
33
Total Activities
31
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Functional
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Prostaglandin E2 receptor EP4 subtype (CHEMBL1836)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Difluorolactam compounds as EP4 receptor-selective agonists for use in the treatment of EP4-mediated diseases and conditions
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 33 9.26 11.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3975743 2 11.00
CHEMBL3937596 2 10.79
CHEMBL3897335 1 10.64
CHEMBL3902065 1 10.42
CHEMBL3895047 1 10.33
CHEMBL3893847 1 10.23
CHEMBL3916499 1 10.10
CHEMBL3891907 1 9.82
CHEMBL3982139 1 9.82
CHEMBL62570 1 9.66
CHEMBL3918816 1 9.62
CHEMBL3955128 1 9.43
CHEMBL3977939 1 9.43
CHEMBL64804 1 9.32
CHEMBL3923027 1 9.21
CHEMBL3949856 1 9.14
CHEMBL3959605 1 8.96
CHEMBL3911081 1 8.30
CHEMBL3973091 1 8.09
CHEMBL3949313 1 7.29
CHEMBL3986266 1 7.21
CHEMBL3966743 1 6.70
CHEMBL3978072 1 -
CHEMBL3900979 1 -
CHEMBL3939998 1 -
CHEMBL3969565 1 -
CHEMBL3945327 1 -
CHEMBL3935235 1 -
CHEMBL3964981 1 -
CHEMBL3982730 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3975743 EC50 = 0.01 nM 11.00
CHEMBL3937596 EC50 = 0.0162 nM 10.79
CHEMBL3897335 EC50 = 0.023 nM 10.64
CHEMBL3902065 EC50 = 0.038 nM 10.42
CHEMBL3895047 EC50 = 0.047 nM 10.33
CHEMBL3893847 EC50 = 0.059 nM 10.23
CHEMBL3916499 EC50 = 0.079 nM 10.10
CHEMBL3982139 EC50 = 0.15 nM 9.82
CHEMBL3891907 EC50 = 0.15 nM 9.82
CHEMBL62570 EC50 = 0.22 nM 9.66
CHEMBL3918816 EC50 = 0.24 nM 9.62
CHEMBL3977939 EC50 = 0.37 nM 9.43
CHEMBL3955128 EC50 = 0.37 nM 9.43
CHEMBL64804 EC50 = 0.48 nM 9.32
CHEMBL3923027 EC50 = 0.61 nM 9.21
CHEMBL3949856 EC50 = 0.73 nM 9.14
CHEMBL3959605 EC50 = 1.1 nM 8.96
CHEMBL3975743 EC50 = 3.15 nM 8.50
CHEMBL3911081 EC50 = 5.02 nM 8.30
CHEMBL3937596 EC50 = 5.68 nM 8.25
CHEMBL3973091 EC50 = 8.09 nM 8.09
CHEMBL3949313 EC50 = 50.8 nM 7.29
CHEMBL3986266 EC50 = 62.0 nM 7.21
CHEMBL3966743 EC50 = 198.0 nM 6.70
CHEMBL3978072 EC50 > 1000.0 nM -
CHEMBL3935235 EC50 > 1000.0 nM -
CHEMBL3939998 EC50 > 1000.0 nM -
CHEMBL3969565 EC50 > 1000.0 nM -
CHEMBL3945327 EC50 = 1.4e-07 nM -
CHEMBL3964981 EC50 > 1000.0 nM -
CHEMBL3982730 EC50 > 1000.0 nM -
CHEMBL3968443 EC50 = 2.7e-06 nM -
CHEMBL3900979 EC50 = 0.0029 nM -