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Assay Detail

CHEMBL3887674

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
High ATP Kinase Assay: For the assay, 50 nl of each stock solution of the test compound in DMSO was pipetted into a black, low-volume 384-well microtiter plate (Greiner Bio-One, Frickenhausen, Germany) 2 μl of a solution of the above FGFR-1 fusion protein in aqueous assay buffer [8 mM MOPS pH 7.0, 10 mM magnesium acetate, 1.0 mM dithiothreitol, 0.05% (w/v) bovine serum albumin (BSA), 0.07% (v/v) Tween-20, 0.2 mM EDTA] was added, and the mixture was incubated for 15 min at 22° C. to allow pre-binding of the test compound to the enzyme. Then, the kinase reaction was started by the addition of 3 ul of a solution of adenosine triphosphate (ATP, 3.3 mM; final concentration in the 5 ul assay volume=2 mM) and substrate (0.16 uM; final concentration in the 5 ul assay volume=0.1 uM) in assay buffer, and the resulting mixture was incubated for a reaction time of 15 min at 22° C. The concentration of FGFR-1 fusion protein was adjusted depending on the activity of the enzyme lot.
123
Total Activities
115
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Fibroblast growth factor receptor 1 (CHEMBL3650)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Disubstituted benzothienyl-pyrrolotriazines and uses thereof
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 123 8.19 9.30

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3951786 1 9.30
CHEMBL3924399 2 9.30
CHEMBL3909132 1 9.15
CHEMBL3892887 1 9.05
CHEMBL3895503 1 9.05
CHEMBL3979384 1 9.05
CHEMBL3985178 1 9.00
CHEMBL3926373 1 9.00
CHEMBL3934668 1 9.00
CHEMBL3905236 1 8.96
CHEMBL3907995 1 8.89
CHEMBL3918062 1 8.89
CHEMBL3937124 1 8.89
CHEMBL3906839 2 8.85
CHEMBL3929322 1 8.85
CHEMBL3938823 1 8.85
CHEMBL3938826 1 8.82
CHEMBL3889953 1 8.80
CHEMBL3938513 1 8.80
CHEMBL3952635 1 8.77
CHEMBL3911335 2 8.72
CHEMBL3984301 1 8.68
CHEMBL3929725 1 8.68
CHEMBL3969060 1 8.68
CHEMBL4108692 1 8.62
CHEMBL3914307 1 8.60
CHEMBL3897839 1 8.57
CHEMBL3958993 1 8.55
CHEMBL3906882 1 8.55
CHEMBL3943773 1 8.55

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3924399 IC50 = 0.5 nM 9.30
CHEMBL3951786 IC50 = 0.5 nM 9.30
CHEMBL3909132 IC50 = 0.7 nM 9.15
CHEMBL3924399 IC50 = 0.7 nM 9.15
CHEMBL3892887 IC50 = 0.9 nM 9.05
CHEMBL3895503 IC50 = 0.9 nM 9.05
CHEMBL3979384 IC50 = 0.9 nM 9.05
CHEMBL3934668 IC50 = 1.0 nM 9.00
CHEMBL3985178 IC50 = 1.0 nM 9.00
CHEMBL3926373 IC50 = 1.0 nM 9.00
CHEMBL3905236 IC50 = 1.1 nM 8.96
CHEMBL3937124 IC50 = 1.3 nM 8.89
CHEMBL3918062 IC50 = 1.3 nM 8.89
CHEMBL3907995 IC50 = 1.3 nM 8.89
CHEMBL3929322 IC50 = 1.4 nM 8.85
CHEMBL3906839 IC50 = 1.4 nM 8.85
CHEMBL3938823 IC50 = 1.4 nM 8.85
CHEMBL3938826 IC50 = 1.5 nM 8.82
CHEMBL3938513 IC50 = 1.6 nM 8.80
CHEMBL3889953 IC50 = 1.6 nM 8.80
CHEMBL3906839 IC50 = 1.7 nM 8.77
CHEMBL3952635 IC50 = 1.7 nM 8.77
CHEMBL3911335 IC50 = 1.9 nM 8.72
CHEMBL3969060 IC50 = 2.1 nM 8.68
CHEMBL3984301 IC50 = 2.1 nM 8.68
CHEMBL3929725 IC50 = 2.1 nM 8.68
CHEMBL4108692 IC50 = 2.4 nM 8.62
CHEMBL3914307 IC50 = 2.5 nM 8.60
CHEMBL3897839 IC50 = 2.7 nM 8.57
CHEMBL3943773 IC50 = 2.8 nM 8.55
CHEMBL3958993 IC50 = 2.8 nM 8.55
CHEMBL3906882 IC50 = 2.8 nM 8.55
CHEMBL3948716 IC50 = 3.0 nM 8.52
CHEMBL3924079 IC50 = 3.1 nM 8.51
CHEMBL3949626 IC50 = 3.2 nM 8.49
CHEMBL3930377 IC50 = 3.2 nM 8.49
CHEMBL3929808 IC50 = 3.3 nM 8.48
CHEMBL3907380 IC50 = 3.4 nM 8.47
CHEMBL3911335 IC50 = 3.4 nM 8.47
CHEMBL3944496 IC50 = 3.7 nM 8.43
CHEMBL3948076 IC50 = 3.7 nM 8.43
CHEMBL3954561 IC50 = 3.8 nM 8.42
CHEMBL3897224 IC50 = 3.9 nM 8.41
CHEMBL3944881 IC50 = 3.9 nM 8.41
CHEMBL3953385 IC50 = 3.9 nM 8.41
CHEMBL3949665 IC50 = 3.9 nM 8.41
CHEMBL3920417 IC50 = 4.0 nM 8.40
CHEMBL3919371 IC50 = 4.1 nM 8.39
CHEMBL4106638 IC50 = 4.2 nM 8.38
CHEMBL3923490 IC50 = 4.2 nM 8.38