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Assay Detail

CHEMBL3888870

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Enzyme Inhibition Assay: The enzyme reaction (total volume 10 μl) was carried out in black 384-well low volume plates containing full length MPS1 (12.5 nM or 3 nM), fluorescent labelled peptide [known as H236, which has the sequence: 5FAM-DHTGFLTEYVATR-CONH2] (5 μM), ATP(10 μM), either DMSO (1% v/v) or the test compound (in the range 0.25 nM-100 μM in 1% DMSO) and assay buffer (50 mM HEPES (pH 7.0), 0.02% NaN3, 0.01% BSA, 0.1 mM Orthovandate, 10 μM MgCl2, 1 μM DTT, Roche protease inhibitor). The reaction was carried out for 60 min at room temperature and stopped by the addition of buffer (10 μl) containing 20 mM EDTA, 0.05% (v/v) Brij-35, in 0.1M HEPES-buffered saline (Free acid, Sigma, UK). The plate was read on a Caliper EZ reader II (Caliper Life Sciences).
205
Total Activities
204
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Dual specificity protein kinase TTK (CHEMBL3983)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Inhibitor compounds
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 205 7.94 9.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3928170 1 9.00
CHEMBL3913772 1 9.00
CHEMBL3919267 1 8.70
CHEMBL3943432 1 8.70
CHEMBL3940708 1 8.70
CHEMBL3946383 1 8.70
CHEMBL3910642 1 8.70
CHEMBL3932996 1 8.70
CHEMBL3890427 1 8.70
CHEMBL3925302 1 8.70
CHEMBL3897889 1 8.70
CHEMBL3919425 1 8.70
CHEMBL3906901 1 8.70
CHEMBL3911468 1 8.70
CHEMBL3962472 1 8.70
CHEMBL3941672 1 8.52
CHEMBL3952394 1 8.52
CHEMBL3908752 1 8.52
CHEMBL3944189 1 8.52
CHEMBL3907282 1 8.52
CHEMBL3901324 1 8.52
CHEMBL3970871 1 8.52
CHEMBL3915042 1 8.52
CHEMBL3941982 1 8.52
CHEMBL3893532 1 8.52
CHEMBL3907465 1 8.52
CHEMBL3939747 1 8.52
CHEMBL3890400 1 8.52
CHEMBL3976598 1 8.52
CHEMBL3930923 1 8.52

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3913772 IC50 = 1.0 nM 9.00
CHEMBL3928170 IC50 = 1.0 nM 9.00
CHEMBL3911468 IC50 = 2.0 nM 8.70
CHEMBL3962472 IC50 = 2.0 nM 8.70
CHEMBL3925302 IC50 = 2.0 nM 8.70
CHEMBL3906901 IC50 = 2.0 nM 8.70
CHEMBL3890427 IC50 = 2.0 nM 8.70
CHEMBL3932996 IC50 = 2.0 nM 8.70
CHEMBL3919267 IC50 = 2.0 nM 8.70
CHEMBL3946383 IC50 = 2.0 nM 8.70
CHEMBL3940708 IC50 = 2.0 nM 8.70
CHEMBL3919425 IC50 = 2.0 nM 8.70
CHEMBL3897889 IC50 = 2.0 nM 8.70
CHEMBL3910642 IC50 = 2.0 nM 8.70
CHEMBL3943432 IC50 = 2.0 nM 8.70
CHEMBL3941982 IC50 = 3.0 nM 8.52
CHEMBL3956274 IC50 = 3.0 nM 8.52
CHEMBL3941672 IC50 = 3.0 nM 8.52
CHEMBL3901423 IC50 = 3.0 nM 8.52
CHEMBL3939747 IC50 = 3.0 nM 8.52
CHEMBL3912889 IC50 = 3.0 nM 8.52
CHEMBL3930923 IC50 = 3.0 nM 8.52
CHEMBL3976598 IC50 = 3.0 nM 8.52
CHEMBL3925962 IC50 = 3.0 nM 8.52
CHEMBL3890400 IC50 = 3.0 nM 8.52
CHEMBL3952394 IC50 = 3.0 nM 8.52
CHEMBL3907428 IC50 = 3.0 nM 8.52
CHEMBL3900773 IC50 = 3.0 nM 8.52
CHEMBL3967187 IC50 = 3.0 nM 8.52
CHEMBL3907465 IC50 = 3.0 nM 8.52
CHEMBL3929386 IC50 = 3.0 nM 8.52
CHEMBL3893532 IC50 = 3.0 nM 8.52
CHEMBL3944189 IC50 = 3.0 nM 8.52
CHEMBL3908752 IC50 = 3.0 nM 8.52
CHEMBL3920481 IC50 = 3.0 nM 8.52
CHEMBL3907282 IC50 = 3.0 nM 8.52
CHEMBL3901324 IC50 = 3.0 nM 8.52
CHEMBL3966905 IC50 = 3.0 nM 8.52
CHEMBL3924132 BOS-172722 IC50 = 3.0 nM 8.52
CHEMBL3917528 IC50 = 3.0 nM 8.52
CHEMBL3970871 IC50 = 3.0 nM 8.52
CHEMBL3915042 IC50 = 3.0 nM 8.52
CHEMBL3951218 IC50 = 4.0 nM 8.40
CHEMBL3972481 IC50 = 4.0 nM 8.40
CHEMBL3958301 IC50 = 4.0 nM 8.40
CHEMBL3956968 IC50 = 4.0 nM 8.40
CHEMBL3955250 IC50 = 4.0 nM 8.40
CHEMBL3943831 IC50 = 4.0 nM 8.40
CHEMBL3986071 IC50 = 4.0 nM 8.40
CHEMBL3934920 IC50 = 4.0 nM 8.40