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Assay Detail

CHEMBL3889239

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Binding
Radioligand Binding Assay: human or rat P2X7-1321 N1 cells were collected and frozen @−80° C. On the day of the experiment, cell membrane preparations were made according to standard published methods. The total assay volume was 100 μl: 10 μl compound (10×)+(b) 40 μl tracer (2.5×)+50 μl membrane (2×). The tracer used for the assay was tritiated A-804598. The compound can be prepared as described in the literature. (Donnelly-Roberts, D. Neuropharmacology 2009, 56 (1), 223-229.) Compounds, tracer and membranes were incubated for 1 hour @ 4° C. The assay was terminated by filtration (GF/B filters pre-soaked with 0.3% PEI) and washed with washing buffer (Tris-HCl 50 mM).
22
Total Activities
22
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

P2X purinoceptor 7 (CHEMBL2496)
Type SINGLE PROTEIN
Organism Rattus norvegicus

Publication

P2X7 modulators
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 22 7.83 8.92

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3919664 1 8.92
CHEMBL4112493 1 8.80
CHEMBL3911720 1 8.70
CHEMBL3954936 1 8.66
CHEMBL4068397 1 8.66
CHEMBL3904992 1 8.60
CHEMBL4113200 1 8.60
CHEMBL4095741 1 8.51
CHEMBL3983427 1 8.49
CHEMBL3951380 1 8.30
CHEMBL4079239 JNJ-54175446 2.0 1 8.26
CHEMBL3937843 1 8.21
CHEMBL3895947 1 8.11
CHEMBL4113942 1 7.85
CHEMBL3924464 1 7.79
CHEMBL3904743 1 7.72
CHEMBL3938984 1 7.58
CHEMBL3901310 1 6.87
CHEMBL3984318 1 6.13
CHEMBL3910103 1 6.10
CHEMBL3923509 1 5.70
CHEMBL4074304 1 5.65

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3919664 Ki = 1.2 nM 8.92
CHEMBL4112493 Ki = 1.6 nM 8.80
CHEMBL3911720 Ki = 2.0 nM 8.70
CHEMBL3954936 Ki = 2.2 nM 8.66
CHEMBL4068397 Ki = 2.2 nM 8.66
CHEMBL3904992 Ki = 2.5 nM 8.60
CHEMBL4113200 Ki = 2.5 nM 8.60
CHEMBL4095741 Ki = 3.1 nM 8.51
CHEMBL3983427 Ki = 3.2 nM 8.49
CHEMBL3951380 Ki = 5.0 nM 8.30
CHEMBL4079239 JNJ-54175446 Ki = 5.5 nM 8.26
CHEMBL3937843 Ki = 6.2 nM 8.21
CHEMBL3895947 Ki = 7.8 nM 8.11
CHEMBL4113942 Ki = 14.1 nM 7.85
CHEMBL3924464 Ki = 16.2 nM 7.79
CHEMBL3904743 Ki = 19.1 nM 7.72
CHEMBL3938984 Ki = 26.3 nM 7.58
CHEMBL3901310 Ki = 134.9 nM 6.87
CHEMBL3984318 Ki = 741.3 nM 6.13
CHEMBL3910103 Ki = 794.3 nM 6.10
CHEMBL3923509 Ki = 1995.3 nM 5.70
CHEMBL4074304 Ki = 2238.7 nM 5.65