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Assay Detail

CHEMBL4008437

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of recombinant human complement factor D catalytic domain (G24 to A253 residues) expressed in Escherichia coli Rosetta using Z-Lys-thiobenzyl as substrate pretreated for 1 hr followed by substrate addition by 2,4-dinitrobenzenesulfonyl-2,7-desmethyl-fluorescein probe based spectrofluorimetric thioesterolysis assay
3
Total Activities
3
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Complement factor D (CHEMBL2176771)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Structure-Based Library Design and Fragment Screening for the Identification of Reversible Complement Factor D Protease Inhibitors.
Vulpetti A, Randl S, Rüdisser S, Ostermann N, Erbel P, Mac Sweeney A, Zoller T, Salem B, Gerhartz B, Cumin F, Hommel U, Dalvit C, Lorthiois E, Maibaum J.
J Med Chem (2017) 60 : 1946 -1958
PubMed 28157311 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 3 4.81 4.85

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4076148 1 4.85
CHEMBL4093577 1 4.77
CHEMBL4065974 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4076148 IC50 = 14000.0 nM 4.85
CHEMBL4093577 IC50 = 17000.0 nM 4.77
CHEMBL4065974 IC50 > 30000.0 nM -