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Assay Detail

CHEMBL4130925

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Irreversible inhibition of recombinant full length His-tagged human BTK expressed in baculovirus expression system using poly (4:1 Glu, Tyr) as substrate preincubated for 2 to 60 mins followed by substrate addition measured after 1 hr by ADP-glo assay
8
Total Activities
4
Compounds Tested
2
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Tyrosine-protein kinase BTK (CHEMBL5251)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Structure-activity relationship investigation for benzonaphthyridinone derivatives as novel potent Bruton's tyrosine kinase (BTK) irreversible inhibitors.
Wang B, Deng Y, Chen Y, Yu K, Wang A, Liang Q, Wang W, Chen C, Wu H, Hu C, Miao W, Hur W, Wang W, Hu Z, Weisberg EL, Wang J, Ren T, Wang Y, Gray NS, Liu Q, Liu J.
Eur J Med Chem (2017) 137 : 545 -557
PubMed 28628824 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 4 8.01 8.70
Kinact 4 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4075449 2 8.70
CHEMBL4091991 2 8.49
CHEMBL4077064 2 7.85
CHEMBL4166664 2 7.01

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4075449 Ki = 2.0 nM 8.70
CHEMBL4091991 Ki = 3.2 nM 8.49
CHEMBL4077064 Ki = 14.2 nM 7.85
CHEMBL4166664 Ki = 97.0 nM 7.01
CHEMBL4075449 Kinact = 0.14 /min -
CHEMBL4166664 Kinact = 0.07 /min -
CHEMBL4091991 Kinact = 0.15 /min -
CHEMBL4077064 Kinact = 0.13 /min -