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Assay Detail

CHEMBL4236563

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Antagonist activity at rat TRPM8 expressed in CHO cells assessed as inhibition of icilin-induced intracellular calcium levels preincubated for 2.5 mins followed by icilin addition by CCD-camera-based FLASH luminometric analysis
9
Total Activities
9
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Rattus norvegicus
Cell Type CHO
Confidence 9 — Direct single protein target
Curated By Autocuration

Publication

Discovery of TRPM8 Antagonist ( S)-6-(((3-Fluoro-4-(trifluoromethoxy)phenyl)(3-fluoropyridin-2-yl)methyl)carbamoyl)nicotinic Acid (AMG 333), a Clinical Candidate for the Treatment of Migraine.
Horne DB, Biswas K, Brown J, Bartberger MD, Clarine J, Davis CD, Gore VK, Harried S, Horner M, Kaller MR, Lehto SG, Liu Q, Ma VV, Monenschein H, Nguyen TT, Yuan CC, Youngblood BD, Zhang M, Zhong W, Allen JR, Chen JJ, Gavva NR.
J Med Chem (2018) 61 : 8186 -8201
PubMed 30148953 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 9 7.77 8.15

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4237618 1 8.15
CHEMBL4243837 1 7.92
CHEMBL4251427 1 7.92
CHEMBL4251467 1 7.89
CHEMBL4241349 1 7.70
CHEMBL4248077 1 7.68
CHEMBL4247840 1 7.68
CHEMBL4250626 1 7.52
CHEMBL4245257 1 7.47

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4237618 IC50 = 7.0 nM 8.15
CHEMBL4243837 IC50 = 12.0 nM 7.92
CHEMBL4251427 IC50 = 12.0 nM 7.92
CHEMBL4251467 IC50 = 13.0 nM 7.89
CHEMBL4241349 IC50 = 20.0 nM 7.70
CHEMBL4248077 IC50 = 21.0 nM 7.68
CHEMBL4247840 IC50 = 21.0 nM 7.68
CHEMBL4250626 IC50 = 30.0 nM 7.52
CHEMBL4245257 IC50 = 34.0 nM 7.47