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Assay Detail

CHEMBL4264020

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of full length human BTK (8 to 80 residues) using FITC-AHA-EEPLYWSFPAKKK-NH2 as substrate after 90 mins by off-chip mobility shift assay
9
Total Activities
9
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Tyrosine-protein kinase BTK (CHEMBL5251)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Optimization of the efflux ratio and permeability of covalent irreversible BTK inhibitors.
Qiu H, Liu-Bujalski L, Caldwell RD, Viacava Follis A, Gardberg A, Goutopoulos A, Grenningloh R, Head J, Johnson T, Jones CCV, Jones R, Mochalkin I, Morandi F, Neagu C, Potnick J, Sherer B.
Bioorg Med Chem Lett (2018) 28 : 3307 -3311
PubMed 30243592 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 9 8.71 9.10

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4288997 1 9.10
CHEMBL4278321 1 8.89
CHEMBL4281335 1 8.89
CHEMBL4245727 1 8.80
CHEMBL4282893 1 8.72
CHEMBL4286628 1 8.66
CHEMBL4278717 1 8.64
CHEMBL4285083 1 8.55
CHEMBL4290066 1 8.12

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4288997 IC50 = 0.8 nM 9.10
CHEMBL4278321 IC50 = 1.3 nM 8.89
CHEMBL4281335 IC50 = 1.3 nM 8.89
CHEMBL4245727 IC50 = 1.6 nM 8.80
CHEMBL4282893 IC50 = 1.9 nM 8.72
CHEMBL4286628 IC50 = 2.2 nM 8.66
CHEMBL4278717 IC50 = 2.3 nM 8.64
CHEMBL4285083 IC50 = 2.8 nM 8.55
CHEMBL4290066 IC50 = 7.5 nM 8.12