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Assay Detail

CHEMBL4264697

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of BTK in goat anti-human IgM F(ab')2-stimulated human PBMC assessed as suppression of BCR-induced CD69 expression on B cells pretreated for 1 hr followed by blood stimulation measured after overnight incubation by flow cytometry
9
Total Activities
9
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type PBMC
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Tyrosine-protein kinase BTK (CHEMBL5251)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Discovery of a novel series of pyridine and pyrimidine carboxamides as potent and selective covalent inhibitors of Btk.
Caldwell R, Liu-Bujalski L, Qiu H, Mochalkin I, Jones R, Neagu C, Goutopoulos A, Grenningloh R, Johnson T, Sherer B, Gardberg A, Follis AV, Morandi F, Head J.
Bioorg Med Chem Lett (2018) 28 : 3419 -3424
PubMed 30290988 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 9 8.09 8.85

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4276669 1 8.85
CHEMBL4279430 1 8.37
CHEMBL1873475 IBRUTINIB 4.0 1 8.34
CHEMBL4279353 1 8.31
CHEMBL4281335 1 8.21
CHEMBL4277875 1 8.15
CHEMBL4285813 1 7.85
CHEMBL4292583 1 7.39
CHEMBL4277754 1 7.36

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4276669 IC50 = 1.4 nM 8.85
CHEMBL4279430 IC50 = 4.3 nM 8.37
CHEMBL1873475 IBRUTINIB IC50 = 4.6 nM 8.34
CHEMBL4279353 IC50 = 4.9 nM 8.31
CHEMBL4281335 IC50 = 6.1 nM 8.21
CHEMBL4277875 IC50 = 7.0 nM 8.15
CHEMBL4285813 IC50 = 14.0 nM 7.85
CHEMBL4292583 IC50 = 41.0 nM 7.39
CHEMBL4277754 IC50 = 44.0 nM 7.36