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Assay Detail

CHEMBL4388992

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Binding
Inhibition of GRP78 (26 to 636 residues) (unknown origin) expressed in Escherichia coli BL21 DE3 cells pre-incubated for 10 mins before FITC-NRLLLTG fluorescent peptide addition in presence of 10 uM ADP followed by further incubation for 2 hrs by fluorescence polarization assay
2
Total Activities
2
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Endoplasmic reticulum chaperone BiP (CHEMBL1781865)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

A high throughput substrate binding assay reveals hexachlorophene as an inhibitor of the ER-resident HSP70 chaperone GRP78.
Ambrose AJ, Zerio CJ, Sivinski J, Schmidlin CJ, Shi T, Ross AB, Widrick KJ, Johnson SM, Zhang DD, Chapman E.
Bioorg Med Chem Lett (2019) 29 : 1689 -1693
PubMed 31129054 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 2 5.57 6.10

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL470334 1 6.10
CHEMBL496 HEXACHLOROPHENE 4.0 1 5.04

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL470334 IC50 = 800.0 nM 6.10
CHEMBL496 HEXACHLOROPHENE IC50 = 9100.0 nM 5.04