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Assay Detail

CHEMBL4394502

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of 20S proteasome beta5 subunit in human RPMI8226 cell lysate using Suc-LLVY-AMC as substrate pretreated for 1 hr followed by substrate addition and measured at 1 min interval by fluorescence assay
9
Total Activities
9
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Subcellular Lysate
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Proteasome Macropain subunit MB1 (CHEMBL4662)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Development of Novel Epoxyketone-Based Proteasome Inhibitors as a Strategy To Overcome Cancer Resistance to Carfilzomib and Bortezomib.
Lee MJ, Bhattarai D, Yoo J, Miller Z, Park JE, Lee S, Lee W, Driscoll JJ, Kim KB.
J Med Chem (2019) 62 : 4444 -4455
PubMed 30964987 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 9 7.61 8.68

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4451741 1 8.68
CHEMBL451887 CARFILZOMIB 4.0 1 8.57
CHEMBL4449204 1 8.10
CHEMBL4532449 1 6.95
CHEMBL4447840 1 5.77
CHEMBL3319605 1 -
CHEMBL4538766 1 -
CHEMBL4529201 1 -
CHEMBL4444547 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4451741 IC50 = 2.1 nM 8.68
CHEMBL451887 CARFILZOMIB IC50 = 2.7 nM 8.57
CHEMBL4449204 IC50 = 8.0 nM 8.10
CHEMBL4532449 IC50 = 111.6 nM 6.95
CHEMBL4447840 IC50 = 1700.0 nM 5.77
CHEMBL3319605 IC50 > 10000.0 nM -
CHEMBL4538766 IC50 > 1000.0 nM -
CHEMBL4529201 IC50 > 1000.0 nM -
CHEMBL4444547 IC50 > 1000.0 nM -