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Assay Detail

CHEMBL4395300

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of recombinant Escherichia coli BL21(DE3) isoleucyl-tRNA synthetase expressed in Escherichia coli Rosetta 2 (DE3) assessed as reduction in tRNA aminoacylation preincubated for 10 mins in presence of [14C]-isoleucin and tRNA followed by ATP addition and measured after 6 mins by scintillation counting method
2
Total Activities
1
Compounds Tested
2
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Escherichia coli BL21(DE3)
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Isoleucine--tRNA ligase (CHEMBL3657)
Type SINGLE PROTEIN
Organism Escherichia coli K-12

Publication

Acylated sulfonamide adenosines as potent inhibitors of the adenylate-forming enzyme superfamily.
De Ruysscher D, Pang L, De Graef S, Nautiyal M, De Borggraeve WM, Rozenski J, Strelkov SV, Weeks SD, Van Aerschot A.
Eur J Med Chem (2019) 174 : 252 -264
PubMed 31048140 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 1 8.92 8.92
IC50 1 8.17 8.17

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4553017 2 8.92

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4553017 Ki = 1.2 nM 8.92
CHEMBL4553017 IC50 = 6.8 nM 8.17