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Assay Detail

CHEMBL4672805

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of BTK in human whole blood assessed as reduction in goat anti human IgM/human IL4-stimulated CD69 cell surface expression on peripheral B cells incubated for 18 hrs by FACS analysis
20
Total Activities
9
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Tissue Blood
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Tyrosine-protein kinase BTK (CHEMBL5251)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Driving Potency with Rotationally Stable Atropisomers: Discovery of Pyridopyrimidinedione-Carbazole Inhibitors of BTK.
Srivastava AS,Ko S,Watterson SH,Pattoli MA,Skala S,Cheng L,Obermeier MT,Vickery R,Discenza LN,D'Arienzo CJ,Gillooly KM,Taylor TL,Pulicicchio C,McIntyre KW,Yip S,Li P,Sun D,Wu DR,Dai J,Wang C,Zhang Y,Wang B,Pawluczyk J,Kempson J,Zhao R,Hou X,Rampulla R,Mathur A,Galella MA,Salter-Cid L,Barrish JC,Carter PH,Fura A,Burke JR,Tino JA
ACS Med Chem Lett (2020) 11 : 2195 -2203
PubMed 33214829 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 20 6.89 7.60

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3928976 4 7.60
CHEMBL3891545 4 7.43
CHEMBL4751952 3 7.16
CHEMBL4743497 3 7.12
CHEMBL4789404 1 6.85
CHEMBL4754459 1 6.85
CHEMBL4741884 2 6.39
CHEMBL3918580 1 6.26
CHEMBL4741099 1 5.52

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3928976 IC50 = 25.0 nM 7.60
CHEMBL3891545 IC50 = 37.0 nM 7.43
CHEMBL3891545 IC50 = 64.0 nM 7.19
CHEMBL4751952 IC50 = 69.0 nM 7.16
CHEMBL4743497 IC50 = 75.0 nM 7.12
CHEMBL4751952 IC50 = 78.0 nM 7.11
CHEMBL4743497 IC50 = 79.0 nM 7.10
CHEMBL4743497 IC50 = 91.0 nM 7.04
CHEMBL4751952 IC50 = 120.0 nM 6.92
CHEMBL4789404 IC50 = 140.0 nM 6.85
CHEMBL4754459 IC50 = 140.0 nM 6.85
CHEMBL3928976 IC50 = 162.0 nM 6.79
CHEMBL4741884 IC50 = 410.0 nM 6.39
CHEMBL3918580 IC50 = 550.0 nM 6.26
CHEMBL4741099 IC50 = 3000.0 nM 5.52
CHEMBL3928976 IC50 - -
CHEMBL3928976 IC50 - -
CHEMBL3891545 IC50 - -
CHEMBL3891545 IC50 - -
CHEMBL4741884 IC50 - -