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Assay Detail

CHEMBL5149645

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of N-terminal His-Smt-tagged MSK1 C-terminal kinase domain (414 to 738 residues) (unknown origin) expressed in Escherichia coli BL21 (DE3) using FAM-PSKPAATRKRRWSAPESR-NH2 as substrate preincubated for 1 hr followed by substrate addition and measured after 70 mins in presence of 250 uM by ADP-Glo kinase assay
5
Total Activities
5
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Ribosomal protein S6 kinase alpha-5 (CHEMBL4237)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Discovery and Characterization of a Novel Series of Chloropyrimidines as Covalent Inhibitors of the Kinase MSK1.
Hall A, Abendroth J, Bolejack MJ, Ceska T, Dell'Aiera S, Ellis V, Fox D, François C, Muruthi MM, Prével C, Poullennec K, Romanov S, Valade A, Vanbellinghen A, Yano J, Geraerts M.
ACS Med Chem Lett (2022) 13 : 1099 -1108
PubMed 35859861 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 5 6.00 6.70

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5186781 1 6.70
CHEMBL5187801 1 6.40
CHEMBL5183977 1 6.10
CHEMBL5208671 1 5.80
CHEMBL5191771 1 5.00

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5186781 IC50 = 199.53 nM 6.70
CHEMBL5187801 IC50 = 398.11 nM 6.40
CHEMBL5183977 IC50 = 794.33 nM 6.10
CHEMBL5208671 IC50 = 1584.89 nM 5.80
CHEMBL5191771 IC50 = 10000.0 nM 5.00