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Assay Detail

CHEMBL5442204

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
PDSP Secondary Binding target: HRH1 - Compounds are tested at 10 uM concentration, plate are incubated at room temperature in the dark for 90 minutes. Reaction are stopped by vacuum filtration onto 0.3% polyethyleneimine soaked filter mats using Filtermate harvester. Scintillation cocktail is then melted onto microwave-dried filters on a hot plate and the radio activity is counted in Microbia counter. Compounds showing a minimum of 50% inhibition at 10 uM concentration are carried forward in this secondary binding assay to determine equilibrium binding affinity.
35
Total Activities
35
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Category PDSP assay
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Histamine H1 receptor (CHEMBL231)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

EUbOPEN Chemogenomics Library - PDSP Secondary Binding
EUbOPEN
(2024)
· DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 35 6.55 8.96

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL1200809 AZELASTINE HYDROCHLORIDE 4.0 1 8.96
CHEMBL1633 KETOTIFEN FUMARATE 4.0 1 8.95
CHEMBL2105760 BREXPIPRAZOLE 4.0 1 8.05
CHEMBL267777 RITANSERIN 2.0 1 7.92
CHEMBL2024517 CARIPRAZINE HYDROCHLORIDE 4.0 1 7.77
CHEMBL3545181 TIOTROPIUM BROMIDE 4.0 1 7.68
CHEMBL83894 FANANSERIN 2.0 1 7.51
CHEMBL405355 NIGULDIPINE 2.0 1 7.05
CHEMBL1200618 FEXOFENADINE HYDROCHLORIDE 4.0 1 7.03
CHEMBL1200492 NEFAZODONE HYDROCHLORIDE 4.0 1 6.90
CHEMBL540612 1 6.90
CHEMBL1722209 TOLTERODINE TARTRATE 4.0 1 6.89
CHEMBL74355 VOLINANSERIN 3.0 1 6.88
CHEMBL3215877 1 6.68
CHEMBL79834 SPIRAMIDE 2.0 1 6.51
CHEMBL1615374 VILAZODONE HYDROCHLORIDE 4.0 1 6.44
CHEMBL5076314 1 6.39
CHEMBL103769 1 6.19
CHEMBL1489369 1 6.12
CHEMBL2107572 TECALCET HYDROCHLORIDE 2.0 1 6.04
CHEMBL2181226 1 5.99
CHEMBL4164059 PITOLISANT HYDROCHLORIDE 4.0 1 5.92
CHEMBL519240 1 5.89
CHEMBL502882 1 5.84
CHEMBL4743049 1 5.84
CHEMBL273083 1 5.79
CHEMBL5075931 1 5.78
CHEMBL494502 1 5.70
CHEMBL24778 SILODOSIN 4.0 1 5.45
CHEMBL1256998 1 5.33

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL1200809 AZELASTINE HYDROCHLORIDE Ki = 1.09 nM 8.96
CHEMBL1633 KETOTIFEN FUMARATE Ki = 1.13 nM 8.95
CHEMBL2105760 BREXPIPRAZOLE Ki = 8.875 nM 8.05
CHEMBL267777 RITANSERIN Ki = 12.17 nM 7.92
CHEMBL2024517 CARIPRAZINE HYDROCHLORIDE Ki = 16.81 nM 7.77
CHEMBL3545181 TIOTROPIUM BROMIDE Ki = 20.8 nM 7.68
CHEMBL83894 FANANSERIN Ki = 30.64 nM 7.51
CHEMBL405355 NIGULDIPINE Ki = 89.66 nM 7.05
CHEMBL1200618 FEXOFENADINE HYDROCHLORIDE Ki = 93.11 nM 7.03
CHEMBL1200492 NEFAZODONE HYDROCHLORIDE Ki = 124.91 nM 6.90
CHEMBL540612 Ki = 125.29 nM 6.90
CHEMBL1722209 TOLTERODINE TARTRATE Ki = 127.37 nM 6.89
CHEMBL74355 VOLINANSERIN Ki = 132.48 nM 6.88
CHEMBL3215877 Ki = 208.55 nM 6.68
CHEMBL79834 SPIRAMIDE Ki = 308.32 nM 6.51
CHEMBL1615374 VILAZODONE HYDROCHLORIDE Ki = 364.46 nM 6.44
CHEMBL5076314 Ki = 402.9 nM 6.39
CHEMBL103769 Ki = 648.63 nM 6.19
CHEMBL1489369 Ki = 760.94 nM 6.12
CHEMBL2107572 TECALCET HYDROCHLORIDE Ki = 908.76 nM 6.04
CHEMBL2181226 Ki = 1014.84 nM 5.99
CHEMBL4164059 PITOLISANT HYDROCHLORIDE Ki = 1200.47 nM 5.92
CHEMBL519240 Ki = 1284.69 nM 5.89
CHEMBL502882 Ki = 1451.44 nM 5.84
CHEMBL4743049 Ki = 1447.11 nM 5.84
CHEMBL273083 Ki = 1614.17 nM 5.79
CHEMBL5075931 Ki = 1647.98 nM 5.78
CHEMBL494502 Ki = 1979.7 nM 5.70
CHEMBL24778 SILODOSIN Ki = 3526.55 nM 5.45
CHEMBL1256998 Ki = 4656.93 nM 5.33
CHEMBL2182029 Ki = 5546.26 nM 5.26
CHEMBL1257131 RAUWOLSCINE HYDROCHLORIDE Ki = 5824.38 nM 5.24
CHEMBL344159 TOLVAPTAN Ki = 6687.29 nM 5.17
CHEMBL1474387 Ki > 10000.0 nM -
CHEMBL3741589 Ki > 10000.0 nM -