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Assay Detail

CHEMBL5730205

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Time Resolved-Fluorescence Resonance Energy Transfer (TR-FRET) Assay: Representative compounds were serially diluted in dimethyl sulfoxide (DMSO) starting at 50 μM (2× starting concentration; 10% DMSO) and 10 μL were transferred into a 384-well plate. Then 10 μL of a protein/probe/antibody mix was added to each well at final concentrations listed in TABLE 1. The samples are then mixed on a shaker for 1 minute and incubated for an additional 3 hours at room temperature. For each assay, the probed antibody and protein/probe/antibody were included on each assay plate as negative and positive controls, respectively. Fluorescence was measured on the Envision (Perkin Elmer) using a 340/35 nm excitation filter and 520/525 (F-Bak peptide) and 495/510 nm (Tb-labeled anti-Histidine antibody) emission filters.
1221
Total Activities
404
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Apoptosis regulator Bcl-2 (CHEMBL4860)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Apoptosis-inducing agents for the treatment of cancer and immune and autoimmune diseases
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 407 9.36 11.00
kon 407 - -
k_off 407 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3653966 3 11.00
CHEMBL3650632 3 10.92
CHEMBL3654125 3 10.92
CHEMBL3650520 3 10.89
CHEMBL3654122 3 10.85
CHEMBL3654127 3 10.85
CHEMBL3654119 3 10.82
CHEMBL3968773 3 10.80
CHEMBL3654111 3 10.80
CHEMBL3654038 3 10.77
CHEMBL3654049 3 10.77
CHEMBL3654099 3 10.77
CHEMBL3654152 3 10.74
CHEMBL3650649 3 10.72
CHEMBL3654107 3 10.72
CHEMBL3650522 3 10.72
CHEMBL3650521 3 10.72
CHEMBL3653975 3 10.70
CHEMBL3654139 3 10.70
CHEMBL3654146 3 10.70
CHEMBL3650617 3 10.68
CHEMBL3650517 3 10.66
CHEMBL3650668 3 10.62
CHEMBL3650523 3 10.57
CHEMBL3653981 3 10.57
CHEMBL3650624 3 10.55
CHEMBL3650637 3 10.55
CHEMBL3654078 3 10.55
CHEMBL3654079 3 10.54
CHEMBL3650524 3 10.52

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3653966 Ki = 0.01 nM 11.00
CHEMBL3650632 Ki = 0.012 nM 10.92
CHEMBL3654125 Ki = 0.012 nM 10.92
CHEMBL3650520 Ki = 0.013 nM 10.89
CHEMBL3654127 Ki = 0.014 nM 10.85
CHEMBL3654122 Ki = 0.014 nM 10.85
CHEMBL3654119 Ki = 0.015 nM 10.82
CHEMBL3968773 Ki = 0.016 nM 10.80
CHEMBL3654111 Ki = 0.016 nM 10.80
CHEMBL3654049 Ki = 0.017 nM 10.77
CHEMBL3654099 Ki = 0.017 nM 10.77
CHEMBL3654038 Ki = 0.017 nM 10.77
CHEMBL3654152 Ki = 0.018 nM 10.74
CHEMBL3650649 Ki = 0.019 nM 10.72
CHEMBL3650522 Ki = 0.019 nM 10.72
CHEMBL3650521 Ki = 0.019 nM 10.72
CHEMBL3654107 Ki = 0.019 nM 10.72
CHEMBL3654139 Ki = 0.02 nM 10.70
CHEMBL3654146 Ki = 0.02 nM 10.70
CHEMBL3653975 Ki = 0.02 nM 10.70
CHEMBL3650617 Ki = 0.021 nM 10.68
CHEMBL3650517 Ki = 0.022 nM 10.66
CHEMBL3650668 Ki = 0.024 nM 10.62
CHEMBL3653981 Ki = 0.027 nM 10.57
CHEMBL3650523 Ki = 0.027 nM 10.57
CHEMBL3654078 Ki = 0.028 nM 10.55
CHEMBL3650637 Ki = 0.028 nM 10.55
CHEMBL3650624 Ki = 0.028 nM 10.55
CHEMBL3654079 Ki = 0.029 nM 10.54
CHEMBL3650524 Ki = 0.03 nM 10.52
CHEMBL3650607 Ki = 0.03 nM 10.52
CHEMBL3654170 Ki = 0.03 nM 10.52
CHEMBL3653978 Ki = 0.031 nM 10.51
CHEMBL3650638 Ki = 0.031 nM 10.51
CHEMBL3650594 Ki = 0.032 nM 10.49
CHEMBL3654120 Ki = 0.033 nM 10.48
CHEMBL3650604 Ki = 0.033 nM 10.48
CHEMBL3654090 Ki = 0.034 nM 10.47
CHEMBL3650525 Ki = 0.034 nM 10.47
CHEMBL3650662 Ki = 0.035 nM 10.46
CHEMBL3650634 Ki = 0.035 nM 10.46
CHEMBL3654159 Ki = 0.035 nM 10.46
CHEMBL3650664 Ki = 0.036 nM 10.44
CHEMBL3650526 Ki = 0.036 nM 10.44
CHEMBL3650655 Ki = 0.036 nM 10.44
CHEMBL3650595 Ki = 0.036 nM 10.44
CHEMBL3650645 Ki = 0.036 nM 10.44
CHEMBL3653971 Ki = 0.037 nM 10.43
CHEMBL3654084 Ki = 0.037 nM 10.43
CHEMBL3653995 Ki = 0.037 nM 10.43