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Assay Detail

CHEMBL5730262

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Kinase-Glo Assay: These assays are set up in duplicate 50 ul volumes in white, flat bottom 96 well plates. Inhibitors are added to the solution of 1× kinase buffer, 10 uM ATP, 100 uM Pim-1-specific substrate, 50 ng of active Pim-1 enzyme, and water in serial dilutions ranging from micromolar to nanomolar concentrations. This solution is incubated at 30 degrees Celsius at 360 rpm for two hours. Following the incubation, 50 ul of Kinase-Glo reagent is added to each well, including all positive and negative control wells, and incubated at room temperature for 15 minutes. The plate is then read by the Luminoskan Ascent instrument and the results displayed with the Ascent Software version 2.6.
312
Total Activities
103
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Serine/threonine-protein kinase pim-1 (CHEMBL2147)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Substituted imidazo[1,2-b]pyridazines as protein kinase inhibitors
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 104 7.11 9.00
kon 104 - -
k_off 104 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3975308 NUVISERTIB 2.0 3 9.00
CHEMBL3928943 3 8.70
CHEMBL3938841 3 8.40
CHEMBL3973281 3 8.40
CHEMBL3947323 3 8.40
CHEMBL3979144 3 8.30
CHEMBL3355542 3 8.30
CHEMBL3964407 3 8.15
CHEMBL3929683 3 8.15
CHEMBL3936197 3 8.10
CHEMBL3976594 3 8.10
CHEMBL3917577 3 8.05
CHEMBL3935594 3 8.00
CHEMBL3951241 3 7.92
CHEMBL3895053 3 7.89
CHEMBL3891871 3 7.89
CHEMBL3965204 3 7.89
CHEMBL3914589 3 7.85
CHEMBL3935431 3 7.85
CHEMBL3976705 3 7.80
CHEMBL3952816 3 7.80
CHEMBL3915263 3 7.77
CHEMBL3355552 3 7.77
CHEMBL3920771 3 7.75
CHEMBL3941934 3 7.75
CHEMBL3943090 3 7.72
CHEMBL3930875 3 7.64
CHEMBL3355987 3 7.64
CHEMBL3355557 6 7.62
CHEMBL3355550 3 7.60

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3975308 NUVISERTIB IC50 = 1.0 nM 9.00
CHEMBL3928943 IC50 = 2.0 nM 8.70
CHEMBL3947323 IC50 = 4.0 nM 8.40
CHEMBL3938841 IC50 = 4.0 nM 8.40
CHEMBL3973281 IC50 = 4.0 nM 8.40
CHEMBL3355542 IC50 = 5.0 nM 8.30
CHEMBL3979144 IC50 = 5.0 nM 8.30
CHEMBL3929683 IC50 = 7.0 nM 8.15
CHEMBL3964407 IC50 = 7.0 nM 8.15
CHEMBL3976594 IC50 = 8.0 nM 8.10
CHEMBL3936197 IC50 = 8.0 nM 8.10
CHEMBL3917577 IC50 = 9.0 nM 8.05
CHEMBL3935594 IC50 = 10.0 nM 8.00
CHEMBL3951241 IC50 = 12.0 nM 7.92
CHEMBL3965204 IC50 = 13.0 nM 7.89
CHEMBL3891871 IC50 = 13.0 nM 7.89
CHEMBL3895053 IC50 = 13.0 nM 7.89
CHEMBL3914589 IC50 = 14.0 nM 7.85
CHEMBL3935431 IC50 = 14.0 nM 7.85
CHEMBL3952816 IC50 = 16.0 nM 7.80
CHEMBL3976705 IC50 = 16.0 nM 7.80
CHEMBL3355552 IC50 = 17.0 nM 7.77
CHEMBL3915263 IC50 = 17.0 nM 7.77
CHEMBL3941934 IC50 = 18.0 nM 7.75
CHEMBL3920771 IC50 = 18.0 nM 7.75
CHEMBL3943090 IC50 = 19.0 nM 7.72
CHEMBL3930875 IC50 = 23.0 nM 7.64
CHEMBL3355987 IC50 = 23.0 nM 7.64
CHEMBL3355557 IC50 = 24.0 nM 7.62
CHEMBL3355557 IC50 = 24.0 nM 7.62
CHEMBL3355550 IC50 = 25.0 nM 7.60
CHEMBL3355544 IC50 = 27.0 nM 7.57
CHEMBL3953965 IC50 = 28.0 nM 7.55
CHEMBL3929768 IC50 = 30.0 nM 7.52
CHEMBL3927091 IC50 = 30.0 nM 7.52
CHEMBL3959607 IC50 = 30.0 nM 7.52
CHEMBL3965060 IC50 = 33.0 nM 7.48
CHEMBL3962567 IC50 = 34.0 nM 7.47
CHEMBL4107503 IC50 = 34.0 nM 7.47
CHEMBL4113689 IC50 = 36.0 nM 7.44
CHEMBL3961837 IC50 = 38.0 nM 7.42
CHEMBL3945649 IC50 = 41.0 nM 7.39
CHEMBL3355541 IC50 = 45.0 nM 7.35
CHEMBL3922142 IC50 = 46.0 nM 7.34
CHEMBL426658 IC50 = 48.0 nM 7.32
CHEMBL3918006 IC50 = 52.0 nM 7.28
CHEMBL3961500 IC50 = 53.0 nM 7.28
CHEMBL3355551 IC50 = 54.0 nM 7.27
CHEMBL3914508 IC50 = 56.0 nM 7.25
CHEMBL3976290 IC50 = 58.0 nM 7.24