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Assay Detail

CHEMBL5730834

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Binding
Radiochemistry Enzymatic Assay: A rat VAP-1 enzyme (SSAO) (reference: Biol Pharm Bull. 2005 March; 28(3): 413-8) activity was measured by a radiochemistry-enzymatic assay using 14C-benzylamine as an artificial substrate. After homogenizing CHO (Chinese Hamster Ovary) cells stably expressing a rat VAP-1 enzyme (SSAO) in a 50 mM phosphate buffer containing 1% NP-40, an enzyme suspension was obtained by taking the supernatant obtained by centrifugation. The enzyme suspension was preincubated with the compound of the present invention in a 96-well microplate at room temperature for 30 minutes. Subsequently, the enzyme suspension was incubated with 14C-benzylamine (a final concentration of 1×10−5 mol/L) to a final volume of 50 mL at 37° C. for 1 hour. The enzymatic reaction was stopped by the addition of 2 mol/L (50 μL) of citric acid. The oxidation products were extracted directly in a 200 μL toluene scintillator, and the radioactivity was measured with a scintillation spectrometer.
114
Total Activities
37
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Amine oxidase [copper-containing] 3 (CHEMBL4592)
Type SINGLE PROTEIN
Organism Rattus norvegicus

Publication

Guanidine compound
(2017)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 38 8.75 9.28
kon 38 - -
k_off 38 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5892320 3 9.28
CHEMBL5816555 6 9.09
CHEMBL6014613 3 9.05
CHEMBL5838951 3 9.02
CHEMBL6014263 3 9.01
CHEMBL5776825 3 9.01
CHEMBL5915647 3 9.00
CHEMBL6011649 3 8.96
CHEMBL5815180 3 8.92
CHEMBL6018287 3 8.92
CHEMBL5741414 3 8.89
CHEMBL5872917 3 8.85
CHEMBL6045381 3 8.85
CHEMBL5929646 3 8.85
CHEMBL5814853 3 8.82
CHEMBL5785705 3 8.82
CHEMBL5847433 3 8.80
CHEMBL5764728 3 8.80
CHEMBL5753110 3 8.77
CHEMBL5957502 3 8.77
CHEMBL5909475 3 8.77
CHEMBL6034079 3 8.74
CHEMBL5996897 3 8.74
CHEMBL5756303 3 8.72
CHEMBL5951266 3 8.72
CHEMBL5877970 3 8.70
CHEMBL5993668 3 8.68
CHEMBL5807211 3 8.66
CHEMBL5940131 3 8.60
CHEMBL6014894 3 8.59

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5892320 IC50 = 0.53 nM 9.28
CHEMBL5816555 IC50 = 0.81 nM 9.09
CHEMBL5816555 IC50 = 0.81 nM 9.09
CHEMBL6014613 IC50 = 0.9 nM 9.05
CHEMBL5838951 IC50 = 0.95 nM 9.02
CHEMBL6014263 IC50 = 0.97 nM 9.01
CHEMBL5776825 IC50 = 0.97 nM 9.01
CHEMBL5915647 IC50 = 1.0 nM 9.00
CHEMBL6011649 IC50 = 1.1 nM 8.96
CHEMBL5815180 IC50 = 1.2 nM 8.92
CHEMBL6018287 IC50 = 1.2 nM 8.92
CHEMBL5741414 IC50 = 1.3 nM 8.89
CHEMBL5929646 IC50 = 1.4 nM 8.85
CHEMBL6045381 IC50 = 1.4 nM 8.85
CHEMBL5872917 IC50 = 1.4 nM 8.85
CHEMBL5785705 IC50 = 1.5 nM 8.82
CHEMBL5814853 IC50 = 1.5 nM 8.82
CHEMBL5764728 IC50 = 1.6 nM 8.80
CHEMBL5847433 IC50 = 1.6 nM 8.80
CHEMBL5957502 IC50 = 1.7 nM 8.77
CHEMBL5753110 IC50 = 1.7 nM 8.77
CHEMBL5909475 IC50 = 1.7 nM 8.77
CHEMBL6034079 IC50 = 1.8 nM 8.74
CHEMBL5996897 IC50 = 1.8 nM 8.74
CHEMBL5756303 IC50 = 1.9 nM 8.72
CHEMBL5951266 IC50 = 1.9 nM 8.72
CHEMBL5877970 IC50 = 2.0 nM 8.70
CHEMBL5993668 IC50 = 2.1 nM 8.68
CHEMBL5807211 IC50 = 2.2 nM 8.66
CHEMBL5940131 IC50 = 2.5 nM 8.60
CHEMBL6014894 IC50 = 2.6 nM 8.59
CHEMBL5757911 IC50 = 3.0 nM 8.52
CHEMBL5985341 IC50 = 3.5 nM 8.46
CHEMBL6020987 IC50 = 3.9 nM 8.41
CHEMBL5778239 IC50 = 4.4 nM 8.36
CHEMBL5917130 IC50 = 5.5 nM 8.26
CHEMBL5772276 IC50 = 6.6 nM 8.18
CHEMBL5909531 IC50 = 22.0 nM 7.66
CHEMBL6014263 k_off = - s-1 -
CHEMBL5741414 kon = - -
CHEMBL5940131 kon = - -
CHEMBL5940131 k_off = - s-1 -
CHEMBL5985341 k_off = - s-1 -
CHEMBL5985341 kon = - -
CHEMBL5816555 kon = - -
CHEMBL5816555 k_off = - s-1 -
CHEMBL5757911 kon = - -
CHEMBL5757911 k_off = - s-1 -
CHEMBL6014263 kon = - -
CHEMBL5815180 kon = - -