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Assay Detail

CHEMBL5730874

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Binding
MAO-B Inhibitory Activity: The MAO-B inhibitory activity evaluation described below followed the protocol of MAO-Glo (registered trademark) Assay of Promega KK.A test compound dissolved in DMSO was added to a reaction solution (100 mM HEPES (pH 7.5), 5% glycerol, 10% DMSO) containing MAO-B enzyme (Sigma-Aldrich Co. LLC.), and the mixture was reacted at room temperature for 15 min. MAO substrate (Promega KK) was added to start the reaction. After reaction at room temperature for 60 min, Luciferine detection reagent (Promega KK) (50 μL) was added to terminate the reaction. After reaction at room temperature for 20 min with stirring, the luminescence was measured by Envision (PerkinElmer). The MAO-B inhibitory rate (%) of the test compound was calculated by the following formula.inhibitory rate (%)=(1−(test compound count−blank)÷(control−blank))×100The count of the MAO-B enzyme reaction mixture under compound non-addition conditions is indicated as control, and the count under compound non-addition and MAO-B enzyme non-addition conditions is indicated as blank. A concentration necessary for achieving 50% inhibitory rate was taken as IC50 value.
375
Total Activities
111
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Amine oxidase [flavin-containing] B (CHEMBL2039)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Cyclopropanamine compound and use thereof
(2018)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 125 4.31 5.22
kon 125 - -
k_off 125 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL6038994 3 5.22
CHEMBL5934359 3 4.64
CHEMBL6044125 3 4.55
CHEMBL6012828 3 4.18
CHEMBL5982091 3 4.06
CHEMBL6016392 3 4.05
CHEMBL6026011 3 4.03
CHEMBL5746541 3 4.02
CHEMBL5849999 3 4.00
CHEMBL5830307 3 -
CHEMBL5931269 3 -
CHEMBL5856046 3 -
CHEMBL5912654 3 -
CHEMBL5781144 3 -
CHEMBL6015466 3 -
CHEMBL5928368 3 -
CHEMBL6052467 3 -
CHEMBL5847679 3 -
CHEMBL5771547 3 -
CHEMBL6024729 3 -
CHEMBL5797523 3 -
CHEMBL5919816 3 -
CHEMBL5747328 3 -
CHEMBL5863242 3 -
CHEMBL5848503 3 -
CHEMBL5957352 3 -
CHEMBL5773232 3 -
CHEMBL5870582 3 -
CHEMBL5880544 6 -
CHEMBL5955351 3 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL6038994 IC50 = 6000.0 nM 5.22
CHEMBL5934359 IC50 = 23000.0 nM 4.64
CHEMBL6044125 IC50 = 28000.0 nM 4.55
CHEMBL6012828 IC50 = 66000.0 nM 4.18
CHEMBL5982091 IC50 = 88000.0 nM 4.06
CHEMBL6016392 IC50 = 90000.0 nM 4.05
CHEMBL6026011 IC50 = 93000.0 nM 4.03
CHEMBL5746541 IC50 = 96000.0 nM 4.02
CHEMBL5849999 IC50 = 100000.0 nM 4.00
CHEMBL6013186 kon = - -
CHEMBL6013186 k_off = - s-1 -
CHEMBL6019623 IC50 > 100000.0 nM -
CHEMBL6019623 kon = - -
CHEMBL6019623 k_off = - s-1 -
CHEMBL5887105 IC50 > 100000.0 nM -
CHEMBL5887105 kon = - -
CHEMBL5887105 k_off = - s-1 -
CHEMBL5947728 k_off = - s-1 -
CHEMBL5824909 IC50 > 100000.0 nM -
CHEMBL6013186 IC50 > 100000.0 nM -
CHEMBL5807170 k_off = - s-1 -
CHEMBL5914875 k_off = - s-1 -
CHEMBL6007489 kon = - -
CHEMBL6007489 k_off = - s-1 -
CHEMBL5807170 IC50 > 100000.0 nM -
CHEMBL5807170 kon = - -
CHEMBL5943902 k_off = - s-1 -
CHEMBL5903914 kon = - -
CHEMBL5903914 IC50 > 100000.0 nM -
CHEMBL5831410 k_off = - s-1 -
CHEMBL6007489 IC50 > 100000.0 nM -
CHEMBL5786983 k_off = - s-1 -
CHEMBL5788357 IC50 > 100000.0 nM -
CHEMBL5788357 kon = - -
CHEMBL5788357 k_off = - s-1 -
CHEMBL3775248 IC50 > 100000.0 nM -
CHEMBL3775248 kon = - -
CHEMBL3775248 k_off = - s-1 -
CHEMBL5831410 IC50 > 100000.0 nM -
CHEMBL5831410 kon = - -
CHEMBL5824909 kon = - -
CHEMBL3775480 IC50 > 100000.0 nM -
CHEMBL3775480 kon = - -
CHEMBL3775480 k_off = - s-1 -
CHEMBL5997734 IC50 > 100000.0 nM -
CHEMBL5997734 kon = - -
CHEMBL5997734 k_off = - s-1 -
CHEMBL5947728 IC50 > 100000.0 nM -
CHEMBL5947728 kon = - -
CHEMBL5903914 k_off = - s-1 -