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Assay Detail

CHEMBL5735651

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Kinase Assay: Briefly, recombinant GSK3β kinase, ATP and Ser/Thr peptide 09 are prepared in 1× Kinase buffer to final concentrations of 0.04 μg/mL, 46 μM, and 4 μM respectively. The mixture is allowed to incubate with the representative compounds for one hour at room temperature. All reactions were performed in duplicate. Unphosphorylated (“0% Control”) and phosphorylated (“100% control”) forms of Ser/Thr 18 serve as control reactions.After incubation, diluted Development Buffer is added to the reaction and allowed to further incubate for one hour at room temperature. The plate is read at Ex 400 Em 455 to detect the coumarin signal and Ex 400 Em 520 to measure the signal (EnVision Multilabel Plate Reader, PerkinElmer).
210
Total Activities
66
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Glycogen synthase kinase-3 beta (CHEMBL262)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

6-(5-membered heteroaryl)isoquinolin-3-yl-(5-membered heteroaryl) carboxamides and preparation and use thereof
(2020)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 70 5.85 8.05
kon 70 - -
k_off 70 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5857120 3 8.05
CHEMBL6000505 3 7.54
CHEMBL5920679 3 6.64
CHEMBL5995698 3 6.54
CHEMBL5792391 3 6.53
CHEMBL5783562 3 6.50
CHEMBL5992147 3 6.49
CHEMBL5854942 3 6.47
CHEMBL4795948 3 6.46
CHEMBL5989365 3 6.41
CHEMBL6018003 3 6.40
CHEMBL4800296 3 6.35
CHEMBL5955685 3 6.34
CHEMBL5996584 3 6.21
CHEMBL6040830 3 6.20
CHEMBL5994578 3 6.19
CHEMBL5927873 3 6.18
CHEMBL5873194 6 6.11
CHEMBL6036161 3 6.11
CHEMBL5782986 3 6.09
CHEMBL5893883 3 6.07
CHEMBL5752492 3 6.01
CHEMBL6045084 6 5.98
CHEMBL5940869 3 5.92
CHEMBL5762477 3 5.90
CHEMBL5886109 3 5.88
CHEMBL5751532 3 5.88
CHEMBL5892413 3 5.87
CHEMBL4787749 3 5.85
CHEMBL6015428 3 5.83

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5857120 EC50 = 9.0 nM 8.05
CHEMBL6000505 EC50 = 29.0 nM 7.54
CHEMBL5920679 EC50 = 230.0 nM 6.64
CHEMBL5995698 EC50 = 286.0 nM 6.54
CHEMBL5792391 EC50 = 295.0 nM 6.53
CHEMBL5783562 EC50 = 316.0 nM 6.50
CHEMBL5992147 EC50 = 322.0 nM 6.49
CHEMBL5854942 EC50 = 342.0 nM 6.47
CHEMBL4795948 EC50 = 349.0 nM 6.46
CHEMBL5989365 EC50 = 390.0 nM 6.41
CHEMBL6018003 EC50 = 395.0 nM 6.40
CHEMBL4800296 EC50 = 450.0 nM 6.35
CHEMBL5955685 EC50 = 458.0 nM 6.34
CHEMBL5996584 EC50 = 611.0 nM 6.21
CHEMBL6040830 EC50 = 628.0 nM 6.20
CHEMBL5994578 EC50 = 641.0 nM 6.19
CHEMBL5927873 EC50 = 666.0 nM 6.18
CHEMBL5873194 EC50 = 769.0 nM 6.11
CHEMBL6036161 EC50 = 780.0 nM 6.11
CHEMBL5782986 EC50 = 821.0 nM 6.09
CHEMBL5893883 EC50 = 850.0 nM 6.07
CHEMBL5873194 EC50 = 979.0 nM 6.01
CHEMBL5752492 EC50 = 986.0 nM 6.01
CHEMBL6045084 EC50 = 1040.0 nM 5.98
CHEMBL5940869 EC50 = 1194.0 nM 5.92
CHEMBL5762477 EC50 = 1263.0 nM 5.90
CHEMBL5886109 EC50 = 1335.0 nM 5.88
CHEMBL5751532 EC50 = 1326.0 nM 5.88
CHEMBL5892413 EC50 = 1350.0 nM 5.87
CHEMBL4787749 EC50 = 1415.0 nM 5.85
CHEMBL4761662 EC50 = 1480.0 nM 5.83
CHEMBL6015428 EC50 = 1495.0 nM 5.83
CHEMBL6024982 EC50 = 1614.0 nM 5.79
CHEMBL6063563 EC50 = 1656.0 nM 5.78
CHEMBL6056650 EC50 = 1655.0 nM 5.78
CHEMBL5784059 EC50 = 1704.0 nM 5.77
CHEMBL4762838 EC50 = 1755.0 nM 5.76
CHEMBL5883539 EC50 = 1769.0 nM 5.75
CHEMBL6038529 EC50 = 1826.0 nM 5.74
CHEMBL5961069 EC50 = 1921.0 nM 5.72
CHEMBL4761662 EC50 = 2063.0 nM 5.69
CHEMBL5929615 EC50 = 2082.0 nM 5.68
CHEMBL6059586 EC50 = 2189.0 nM 5.66
CHEMBL5953637 EC50 = 2179.0 nM 5.66
CHEMBL6035523 EC50 = 2339.0 nM 5.63
CHEMBL4762553 EC50 = 2586.0 nM 5.59
CHEMBL5957402 EC50 = 2747.0 nM 5.56
CHEMBL6056931 EC50 = 2934.0 nM 5.53
CHEMBL5783383 EC50 = 3058.0 nM 5.51
CHEMBL4755579 EC50 = 3071.0 nM 5.51