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Assay Detail

CHEMBL5736211

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Enzyme Assay: The total volume of the ATG7 enzymatic assay is 50 μL and contains 50 mM HEPES Hemisodium (pH 7.5), 0.05% BSA, 0.01% Tween-20, 25 mM NaCl, 5 mM MgCl2, 10 μM ATP, 250 μM GSH, 5 nM ATG3-GST, 5 nM Flag-Gabarap, 100 μM TCEP and 0.15 nM recombinant human His-ATG7 enzyme. The enzymatic reaction mixture, with and without inhibitor, was incubated at 24° C. for 105 min in a 384-well plate before termination with 25 μM of Stop/Detection buffer (0.1M HEPES Hemisodium pH 7.5, 0.05% Tween20, 20 mM EDTA, 410 mM KF, 0.53 nM Europium-Cryptate labeled monoclonal anti-Flag M2 Antibody (CisBio International) and 8.125 μg/ml PHYCOLINK goat anti-GST allophycocyanin (XL-APC) antibody (Prozyme)). After incubation for 2 hours at 24° C., quantification of FRET is performed on the Pherostar (BMG Labtech). Percentage inhibition values at a single concentration or enzyme inhibition (IC50) values are determined from those curves. One skilled in the art will appreciate that the values generated either as percentage inhibition at a single concentration or IC50 values are subject to experimental variation.
693
Total Activities
229
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Ubiquitin-like modifier-activating enzyme ATG7 (CHEMBL2321621)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

ATG7 inhibitors and the uses thereof
(2020)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 231 7.05 7.46
kon 231 - -
k_off 231 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4465490 3 7.46
CHEMBL4449861 3 7.46
CHEMBL5801088 3 7.46
CHEMBL4521754 3 7.46
CHEMBL4535927 3 7.46
CHEMBL4579107 3 7.46
CHEMBL4577562 3 7.46
CHEMBL4476015 3 7.46
CHEMBL4451885 3 7.46
CHEMBL4439106 3 7.46
CHEMBL4531796 3 7.46
CHEMBL4471670 3 7.46
CHEMBL4473245 3 7.46
CHEMBL4453903 3 7.46
CHEMBL4548069 3 7.46
CHEMBL4450880 3 7.46
CHEMBL4539952 3 7.46
CHEMBL4476094 3 7.46
CHEMBL4586427 3 7.46
CHEMBL4455332 3 7.46
CHEMBL4589701 3 7.46
CHEMBL4551253 3 7.46
CHEMBL4529186 3 7.46
CHEMBL4532634 3 7.46
CHEMBL4517771 3 7.46
CHEMBL4574054 3 7.46
CHEMBL4545152 3 7.46
CHEMBL4551395 3 7.46
CHEMBL4436997 3 7.46
CHEMBL4542158 3 7.46

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4452757 IC50 = 35.0 nM 7.46
CHEMBL4449861 IC50 = 35.0 nM 7.46
CHEMBL4551253 IC50 = 35.0 nM 7.46
CHEMBL4466430 IC50 = 35.0 nM 7.46
CHEMBL4543610 IC50 = 35.0 nM 7.46
CHEMBL4589701 IC50 = 35.0 nM 7.46
CHEMBL4549926 IC50 = 35.0 nM 7.46
CHEMBL4455332 IC50 = 35.0 nM 7.46
CHEMBL4521754 IC50 = 35.0 nM 7.46
CHEMBL4557103 IC50 = 35.0 nM 7.46
CHEMBL4439106 IC50 = 35.0 nM 7.46
CHEMBL4557469 IC50 = 35.0 nM 7.46
CHEMBL4586427 IC50 = 35.0 nM 7.46
CHEMBL4576658 IC50 = 35.0 nM 7.46
CHEMBL4475447 IC50 = 35.0 nM 7.46
CHEMBL4476094 IC50 = 35.0 nM 7.46
CHEMBL4539952 IC50 = 35.0 nM 7.46
CHEMBL4453903 IC50 = 35.0 nM 7.46
CHEMBL4526319 IC50 = 35.0 nM 7.46
CHEMBL4589617 IC50 = 35.0 nM 7.46
CHEMBL4518269 IC50 = 35.0 nM 7.46
CHEMBL4518410 IC50 = 35.0 nM 7.46
CHEMBL4476516 IC50 = 35.0 nM 7.46
CHEMBL5927711 IC50 = 35.0 nM 7.46
CHEMBL4471670 IC50 = 35.0 nM 7.46
CHEMBL4558671 IC50 = 35.0 nM 7.46
CHEMBL4476015 IC50 = 35.0 nM 7.46
CHEMBL4551395 IC50 = 35.0 nM 7.46
CHEMBL4545152 IC50 = 35.0 nM 7.46
CHEMBL4436997 IC50 = 35.0 nM 7.46
CHEMBL5801088 IC50 = 35.0 nM 7.46
CHEMBL4464322 IC50 = 35.0 nM 7.46
CHEMBL4449596 IC50 = 35.0 nM 7.46
CHEMBL4517065 IC50 = 35.0 nM 7.46
CHEMBL4574054 IC50 = 35.0 nM 7.46
CHEMBL4483085 IC50 = 35.0 nM 7.46
CHEMBL4444895 IC50 = 35.0 nM 7.46
CHEMBL4451885 IC50 = 35.0 nM 7.46
CHEMBL4577562 IC50 = 35.0 nM 7.46
CHEMBL4542158 IC50 = 35.0 nM 7.46
CHEMBL4469119 IC50 = 35.0 nM 7.46
CHEMBL4471077 IC50 = 35.0 nM 7.46
CHEMBL4469589 IC50 = 35.0 nM 7.46
CHEMBL4467807 IC50 = 35.0 nM 7.46
CHEMBL4517771 IC50 = 35.0 nM 7.46
CHEMBL4457043 IC50 = 35.0 nM 7.46
CHEMBL4532634 IC50 = 35.0 nM 7.46
CHEMBL4447381 IC50 = 35.0 nM 7.46
CHEMBL4454053 IC50 = 35.0 nM 7.46
CHEMBL4529186 IC50 = 35.0 nM 7.46