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Assay Detail

CHEMBL5737550

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Binding
LanthaScreen Eu Kinase Binding Assay: FMS: IC50 values of compounds against FMS kinase were determined by LanthaScreen™ Eu Kinase Binding Assay at Invitrogen (Life Technologies Grand Island, N.Y.) where total reaction volume was 10 μL in low-volume 384-well plates (#4511, Corning). Serially diluted compounds (3-fold) were incubated with kinase (1.25 nM) for 10 min, following which a mixture of ATP (10 μM) (#A1852, Sigma, St-Louis, Mo.) and fluorescent-PolyGT substrate (200 nM) (#PV3610, Invitrogen, Life Technologies Grand Island, N.Y.) was added and incubated in dark at room temperature for 1 h. After 1 h, 10 μL stop solution containing Terbium labeled antibody (4 nM) (#PV3529, Invitrogen, Life Technologies Grand Island, N.Y.) and EDTA (#E5134, Sigma, St-Louis, Mo.) (20 mM) in TR-FRET dilution buffer (#PV3574, Invitrogen, Life Technologies Grand Island, N.Y.) was added. Readings were taken in a Synergy Neo Plate reader (BioTek, Winooski) at single excitation of 340 nm and Dual emission at 495 nm and 520 nm respectively.
285
Total Activities
95
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Macrophage colony-stimulating factor 1 receptor (CHEMBL1844)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Heterocyclic compounds as kinase inhibitors
(2021)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 95 7.28 8.82
kon 95 - -
k_off 95 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5951978 3 8.82
CHEMBL5956531 3 8.70
CHEMBL5996434 3 8.60
CHEMBL5945809 3 8.60
CHEMBL5944626 3 8.60
CHEMBL5861777 3 8.60
CHEMBL6059314 3 8.52
CHEMBL6043217 3 8.52
CHEMBL5782876 3 8.40
CHEMBL5875698 3 8.30
CHEMBL6058548 3 8.30
CHEMBL5770062 3 8.30
CHEMBL5887566 3 8.22
CHEMBL5740706 3 8.19
CHEMBL5877068 3 8.15
CHEMBL6034655 3 8.12
CHEMBL6013201 3 8.10
CHEMBL5858807 3 8.10
CHEMBL6023260 3 8.02
CHEMBL5961536 3 7.85
CHEMBL5997157 3 7.85
CHEMBL5907786 3 7.85
CHEMBL5942169 3 7.77
CHEMBL5843565 3 7.77
CHEMBL5746967 3 7.77
CHEMBL5992232 3 7.75
CHEMBL5876164 3 7.72
CHEMBL5914936 3 7.68
CHEMBL5934647 3 7.66
CHEMBL5976864 3 7.62

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5951978 IC50 = 1.5 nM 8.82
CHEMBL5956531 IC50 = 2.0 nM 8.70
CHEMBL5996434 IC50 = 2.5 nM 8.60
CHEMBL5944626 IC50 = 2.5 nM 8.60
CHEMBL5861777 IC50 = 2.5 nM 8.60
CHEMBL5945809 IC50 = 2.5 nM 8.60
CHEMBL6059314 IC50 = 3.0 nM 8.52
CHEMBL6043217 IC50 = 3.0 nM 8.52
CHEMBL5782876 IC50 = 4.0 nM 8.40
CHEMBL6058548 IC50 = 5.0 nM 8.30
CHEMBL5770062 IC50 = 5.0 nM 8.30
CHEMBL5875698 IC50 = 5.0 nM 8.30
CHEMBL5887566 IC50 = 6.0 nM 8.22
CHEMBL5740706 IC50 = 6.5 nM 8.19
CHEMBL5877068 IC50 = 7.0 nM 8.15
CHEMBL6034655 IC50 = 7.5 nM 8.12
CHEMBL5858807 IC50 = 8.0 nM 8.10
CHEMBL6013201 IC50 = 8.0 nM 8.10
CHEMBL6023260 IC50 = 9.5 nM 8.02
CHEMBL5907786 IC50 = 14.0 nM 7.85
CHEMBL5961536 IC50 = 14.0 nM 7.85
CHEMBL5997157 IC50 = 14.0 nM 7.85
CHEMBL5843565 IC50 = 17.0 nM 7.77
CHEMBL5746967 IC50 = 17.0 nM 7.77
CHEMBL5942169 IC50 = 17.0 nM 7.77
CHEMBL5992232 IC50 = 18.0 nM 7.75
CHEMBL5876164 IC50 = 19.0 nM 7.72
CHEMBL5914936 IC50 = 21.0 nM 7.68
CHEMBL5934647 IC50 = 22.0 nM 7.66
CHEMBL5976864 IC50 = 24.0 nM 7.62
CHEMBL5917565 IC50 = 25.0 nM 7.60
CHEMBL5774057 IC50 = 25.0 nM 7.60
CHEMBL6049510 IC50 = 28.0 nM 7.55
CHEMBL5803114 IC50 = 29.0 nM 7.54
CHEMBL5758578 IC50 = 29.0 nM 7.54
CHEMBL5877196 IC50 = 33.0 nM 7.48
CHEMBL5822252 IC50 = 35.0 nM 7.46
CHEMBL5887109 IC50 = 36.0 nM 7.44
CHEMBL5760232 IC50 = 40.0 nM 7.40
CHEMBL5899619 IC50 = 42.0 nM 7.38
CHEMBL6052625 IC50 = 42.0 nM 7.38
CHEMBL6045551 IC50 = 46.0 nM 7.34
CHEMBL5955040 IC50 = 48.0 nM 7.32
CHEMBL5965360 IC50 = 49.0 nM 7.31
CHEMBL5869636 IC50 = 49.0 nM 7.31
CHEMBL5792947 IC50 = 58.0 nM 7.24
CHEMBL5779951 IC50 = 61.0 nM 7.21
CHEMBL5968635 IC50 = 66.0 nM 7.18
CHEMBL5996998 IC50 = 68.0 nM 7.17
CHEMBL6012324 IC50 = 67.0 nM 7.17