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Assay Detail

CHEMBL5738846

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Binding
PI3-Kinase HTRF™ Assay: PI3 Kinase α, β, γ or δ activity was assayed using the PI3 Kinase HTRF® assay kit (catalogue No. 33-016) purchased from Millipore Corporation. Purified recombinant PI3Kα (catalogue No. 14-602-K), PI3Kβ (catalogue No. 14-603-K), PI3Kγ (catalogue No. 14-558-K), and PI3Kδ (catalogue No. 14-604-K) were obtained from Millipore Corporation. Purified recombinant PI3K enzyme was used to catalyze the phosphorylation of phosphatidylinositol 4,5-bisphosphate (PIP2 at 10 μM) to phosphatidylinositol 3,4,5-trisphosphate (PIP3) in the presence of 10 μM ATP. The assay was carried out in 384-well format and detected using a Perkin Elmer EnVision Xcite Multilabel Reader. Emission ratios were converted into percent inhibitions and imported into GraphPad Prism software. The concentration necessary to achieve inhibition of enzyme activity by 50% (IC50) was calculated using concentrations ranging from 20 μM to 0.1 nM (12-point curve).
330
Total Activities
108
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Publication

Heterocyclic compounds and uses thereof
(2023)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 110 5.70 5.70
kon 110 - -
k_off 110 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5949875 3 5.70
CHEMBL3914602 3 5.70
CHEMBL5919053 3 5.70
CHEMBL6050868 3 5.70
CHEMBL5900412 3 5.70
CHEMBL3955769 3 5.70
CHEMBL6033616 3 5.70
CHEMBL5871827 3 5.70
CHEMBL5901746 3 5.70
CHEMBL5882857 3 5.70
CHEMBL5886457 3 5.70
CHEMBL5992887 3 5.70
CHEMBL5900338 3 5.70
CHEMBL5953253 3 5.70
CHEMBL3928146 3 5.70
CHEMBL5797332 6 5.70
CHEMBL5785381 3 5.70
CHEMBL5867632 3 5.70
CHEMBL5990604 3 5.70
CHEMBL5754601 3 5.70
CHEMBL5934604 3 5.70
CHEMBL6020506 3 5.70
CHEMBL5915872 3 5.70
CHEMBL5798011 3 5.70
CHEMBL5790749 3 5.70
CHEMBL5925877 3 5.70
CHEMBL3966879 3 5.70
CHEMBL6025507 3 5.70
CHEMBL5766735 3 5.70
CHEMBL6013643 3 5.70

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5829946 IC50 = 2000.0 nM 5.70
CHEMBL6007856 IC50 = 2000.0 nM 5.70
CHEMBL3921445 IC50 = 2000.0 nM 5.70
CHEMBL5791000 IC50 = 2000.0 nM 5.70
CHEMBL5970890 IC50 = 2000.0 nM 5.70
CHEMBL5796536 IC50 = 2000.0 nM 5.70
CHEMBL5895414 IC50 = 2000.0 nM 5.70
CHEMBL5887753 IC50 = 2000.0 nM 5.70
CHEMBL5947378 IC50 = 2000.0 nM 5.70
CHEMBL5806739 IC50 = 2000.0 nM 5.70
CHEMBL5900898 IC50 = 2000.0 nM 5.70
CHEMBL5748222 IC50 = 2000.0 nM 5.70
CHEMBL5762937 IC50 = 2000.0 nM 5.70
CHEMBL5754944 IC50 = 2000.0 nM 5.70
CHEMBL5796587 IC50 = 2000.0 nM 5.70
CHEMBL3895629 IC50 = 2000.0 nM 5.70
CHEMBL6048456 IC50 = 2000.0 nM 5.70
CHEMBL5935134 IC50 = 2000.0 nM 5.70
CHEMBL5858536 IC50 = 2000.0 nM 5.70
CHEMBL5838632 IC50 = 2000.0 nM 5.70
CHEMBL5979518 IC50 = 2000.0 nM 5.70
CHEMBL5743380 IC50 = 2000.0 nM 5.70
CHEMBL5933124 IC50 = 2000.0 nM 5.70
CHEMBL5991752 IC50 = 2000.0 nM 5.70
CHEMBL6021741 IC50 = 2000.0 nM 5.70
CHEMBL3893430 IC50 = 2000.0 nM 5.70
CHEMBL5754507 IC50 = 2000.0 nM 5.70
CHEMBL6033616 IC50 = 2000.0 nM 5.70
CHEMBL3955769 IC50 = 2000.0 nM 5.70
CHEMBL5799818 IC50 = 2000.0 nM 5.70
CHEMBL5900412 IC50 = 2000.0 nM 5.70
CHEMBL6052455 IC50 = 2000.0 nM 5.70
CHEMBL6050868 IC50 = 2000.0 nM 5.70
CHEMBL5919053 IC50 = 2000.0 nM 5.70
CHEMBL5866941 IC50 = 2000.0 nM 5.70
CHEMBL3914602 IC50 = 2000.0 nM 5.70
CHEMBL5764062 IC50 = 2000.0 nM 5.70
CHEMBL5760298 IC50 = 2000.0 nM 5.70
CHEMBL5980508 IC50 = 2000.0 nM 5.70
CHEMBL5936480 IC50 = 2000.0 nM 5.70
CHEMBL5996366 IC50 = 2000.0 nM 5.70
CHEMBL5977085 IC50 = 2000.0 nM 5.70
CHEMBL6011851 IC50 = 2000.0 nM 5.70
CHEMBL6011851 IC50 = 2000.0 nM 5.70
CHEMBL5924108 IC50 = 2000.0 nM 5.70
CHEMBL5748405 IC50 = 2000.0 nM 5.70
CHEMBL5971164 IC50 = 2000.0 nM 5.70
CHEMBL6053354 IC50 = 2000.0 nM 5.70
CHEMBL5770638 IC50 = 2000.0 nM 5.70
CHEMBL5776869 IC50 = 2000.0 nM 5.70