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Assay Detail

CHEMBL2339922

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Functional
Agonist activity at human TGR5 expressed in deoxycycline-induced Flp-In-CHO-TO cells assessed as increase in intracellular cAMP measured after 48 hrs by HTRF competitive immunoassay
17
Total Activities
17
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Functional
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

G-protein coupled bile acid receptor 1 (CHEMBL5409)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Identification of Tetrahydropyrido[4,3-d]pyrimidine Amides as a New Class of Orally Bioavailable TGR5 Agonists.
Piotrowski DW, Futatsugi K, Warmus JS, Orr ST, Freeman-Cook KD, Londregan AT, Wei L, Jennings SM, Herr M, Coffey SB, Jiao W, Storer G, Hepworth D, Wang J, Lavergne SY, Chin JE, Hadcock JR, Brenner MB, Wolford AC, Janssen AM, Roush NS, Buxton J, Hinchey T, Kalgutkar AS, Sharma R, Flynn DA.
ACS Med Chem Lett (2013) 4 : 63 -68
PubMed 24900564 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 17 7.83 8.80

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL2331649 1 8.80
CHEMBL2331653 1 8.70
CHEMBL2331648 1 8.64
CHEMBL2331646 1 8.60
CHEMBL2331651 1 8.57
CHEMBL2331655 1 8.55
CHEMBL2331654 1 8.48
CHEMBL2331650 1 8.33
CHEMBL2331645 1 8.04
CHEMBL576138 1 7.62
CHEMBL2331652 1 7.37
CHEMBL604131 1 7.33
CHEMBL2331644 1 7.11
CHEMBL2331647 1 6.86
CHEMBL1258423 1 6.81
CHEMBL567640 1 6.78
CHEMBL2331643 1 6.59

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL2331649 EC50 = 1.6 nM 8.80
CHEMBL2331653 EC50 = 2.0 nM 8.70
CHEMBL2331648 EC50 = 2.3 nM 8.64
CHEMBL2331646 EC50 = 2.5 nM 8.60
CHEMBL2331651 EC50 = 2.7 nM 8.57
CHEMBL2331655 EC50 = 2.8 nM 8.55
CHEMBL2331654 EC50 = 3.3 nM 8.48
CHEMBL2331650 EC50 = 4.7 nM 8.33
CHEMBL2331645 EC50 = 9.2 nM 8.04
CHEMBL576138 EC50 = 24.0 nM 7.62
CHEMBL2331652 EC50 = 43.0 nM 7.37
CHEMBL604131 EC50 = 47.0 nM 7.33
CHEMBL2331644 EC50 = 78.0 nM 7.11
CHEMBL2331647 EC50 = 137.0 nM 6.86
CHEMBL1258423 EC50 = 154.0 nM 6.81
CHEMBL567640 EC50 = 166.0 nM 6.78
CHEMBL2331643 EC50 = 257.0 nM 6.59