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Assay Detail

CHEMBL3431446

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Functional
GSK_TCAKS: pIC50 Trypanosoma cruzi viability assay using beta-GAL activity. This assay was run at single shot at 5uM compound concentration per well. The biological reagents consisted of NIH-3T3 host cells and trypomastigotes parasitic cells; both cell types were set to a 3.3 * 10^5 cells/mL dilution in assay DMEM by means of a CASY cell counter device using a 60um capillary. 6 uL of the mixture were dispensed per well (about 1 * 10^3 host-cells and 1 * 10^3 parasites) with a Multidrop Combi dispenser. Previously, a solution of 1.67 * 10^5 trypomastigotes per mL in assay DMEM had been prepared and 6uL per well dispensed in the allotted control columns that defined 100% inhibition. The 0% inhibition of parasitic growth control was obtained by leaving the assay mixture untreated in its corresponding plate columns. In all wells, the percentage of DMSO never exceeded 0.5%. Plates incubated for four days at 37C, 5% CO2. The substrate used for the assay fluorescence intensity (FLINT) readout was resorufin-beta-D-galactopiranoside (Sigma-Aldrich) at 5uM per well. It was diluted in PBS supplemented with the soft detergent Igepal (Fluka). Upon addition to the plates, the substrate solution was incubated for 4h at room temperature and the signal read with the EnVision microtiter plate reader (Perkin-Elmer) using the corresponding set of filters (excitation/emission at 531/595nm).
584
Total Activities
584
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Functional
Organism Mus musculus
Cell Type NIH3T3
Confidence 1 — Organism
Curated By Autocuration

Target

Trypanosoma cruzi (CHEMBL368)
Type ORGANISM
Organism Trypanosoma cruzi

Publication

GSK Tres Cantos Anti-Kinetoplastid Screening (TCAKS) Data.
Imanol Pena, M. Pilar Manzano, Juan Cantizani, Albane Kessler, Julio Alonso-Padilla, Ana I. Bardera, Emilio Alvarez, Gonzalo Colmenarejo, Ignacio Cotillo, Irene Roquero, Francisco de Dios-Anton, Vanessa Barroso, Ana Rodriguez, David W. Gray, Miguel Navarro, Vinod Kumar, Alexander Sherstnev, David Drewry, James R. Brown, Jose M. Fiandor & J. Julio Martin.

· DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 584 5.92 8.20

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL528583 1 8.20
CHEMBL3431117 1 7.80
CHEMBL3431025 1 7.70
CHEMBL3431261 1 7.70
CHEMBL3431266 1 7.70
CHEMBL3431326 1 7.60
CHEMBL3431435 1 7.60
CHEMBL3431128 1 7.50
CHEMBL3431155 1 7.50
CHEMBL3431368 1 7.40
CHEMBL1325144 1 7.40
CHEMBL3431434 1 7.40
CHEMBL3431140 1 7.30
CHEMBL3431433 1 7.30
CHEMBL3431318 1 7.25
CHEMBL3431129 1 7.20
CHEMBL3430960 1 7.15
CHEMBL3431003 1 7.15
CHEMBL3431257 1 7.15
CHEMBL3431130 1 7.10
CHEMBL3431192 1 7.10
CHEMBL3431206 1 7.10
CHEMBL3431291 1 7.10
CHEMBL3431381 1 7.10
CHEMBL3431029 1 7.00
CHEMBL1458931 1 7.00
CHEMBL3431238 1 7.00
CHEMBL3431354 1 7.00
CHEMBL3431376 1 7.00
CHEMBL3431400 1 7.00

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL528583 IC50 = 6.31 nM 8.20
CHEMBL3431117 IC50 = 15.85 nM 7.80
CHEMBL3431261 IC50 = 19.95 nM 7.70
CHEMBL3431266 IC50 = 19.95 nM 7.70
CHEMBL3431025 IC50 = 19.95 nM 7.70
CHEMBL3431435 IC50 = 25.12 nM 7.60
CHEMBL3431326 IC50 = 25.12 nM 7.60
CHEMBL3431155 IC50 = 31.62 nM 7.50
CHEMBL3431128 IC50 = 31.62 nM 7.50
CHEMBL1325144 IC50 = 39.81 nM 7.40
CHEMBL3431368 IC50 = 39.81 nM 7.40
CHEMBL3431434 IC50 = 39.81 nM 7.40
CHEMBL3431140 IC50 = 50.12 nM 7.30
CHEMBL3431433 IC50 = 50.12 nM 7.30
CHEMBL3431318 IC50 = 56.23 nM 7.25
CHEMBL3431129 IC50 = 63.1 nM 7.20
CHEMBL3431257 IC50 = 70.79 nM 7.15
CHEMBL3430960 IC50 = 70.79 nM 7.15
CHEMBL3431003 IC50 = 70.79 nM 7.15
CHEMBL3431192 IC50 = 79.43 nM 7.10
CHEMBL3431206 IC50 = 79.43 nM 7.10
CHEMBL3431381 IC50 = 79.43 nM 7.10
CHEMBL3431291 IC50 = 79.43 nM 7.10
CHEMBL3431130 IC50 = 79.43 nM 7.10
CHEMBL3431354 IC50 = 100.0 nM 7.00
CHEMBL3431376 IC50 = 100.0 nM 7.00
CHEMBL3431400 IC50 = 100.0 nM 7.00
CHEMBL3431238 IC50 = 100.0 nM 7.00
CHEMBL3431029 IC50 = 100.0 nM 7.00
CHEMBL1458931 IC50 = 100.0 nM 7.00
CHEMBL3431028 IC50 = 112.2 nM 6.95
CHEMBL487186 TEBUCONAZOLE IC50 = 125.89 nM 6.90
CHEMBL3431337 IC50 = 125.89 nM 6.90
CHEMBL3431338 IC50 = 125.89 nM 6.90
CHEMBL3431004 IC50 = 125.89 nM 6.90
CHEMBL2441267 IC50 = 125.89 nM 6.90
CHEMBL3431405 IC50 = 125.89 nM 6.90
CHEMBL3431289 IC50 = 125.89 nM 6.90
CHEMBL3430915 IC50 = 125.89 nM 6.90
CHEMBL3431193 IC50 = 125.89 nM 6.90
CHEMBL3431263 IC50 = 125.89 nM 6.90
CHEMBL3431133 IC50 = 125.89 nM 6.90
CHEMBL3431151 IC50 = 125.89 nM 6.90
CHEMBL3431220 IC50 = 125.89 nM 6.90
CHEMBL3430980 IC50 = 125.89 nM 6.90
CHEMBL3431375 IC50 = 141.25 nM 6.85
CHEMBL3431408 IC50 = 141.25 nM 6.85
CHEMBL1232777 FORMYCIN B IC50 = 141.25 nM 6.85
CHEMBL3431107 IC50 = 141.25 nM 6.85
CHEMBL3431331 IC50 = 141.25 nM 6.85