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Assay Detail

CHEMBL3706152

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Enzyme Inhibition Assay: An IMAP TR-FRET assay was used to analyze the enzyme activity (Molecular Devices Corp., Sunnyvale Calif.). 5 μL of serial diluted PDE10A (BPS Bioscience, San Diego, Calif.) or tissue homogenate was incubated with equal volumes of diluted fluorescein labeled cAMP or cGMP for 60 min in 384-well polystyrene assay plates (Corning, Corning, N.Y.) at room temperature. After incubation, the reaction was stopped by adding 60 μL of diluted binding reagents and was incubated for 3 hours to overnight at room temperature. The plates were read on an Envision (Perkin Elmer, Waltham, Mass.) for time resolved fluorescence resonance energy transfer.
360
Total Activities
351
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Rattus norvegicus
Confidence 9 — Direct single protein target
Curated By Autocuration

Publication

Aminopyridine and carboxypyridine compounds as phosphodiesterase 10 inhibitors
(2014)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 360 7.12 10.40

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3660647 3 10.40
CHEMBL2180802 1 10.35
CHEMBL3660644 1 10.26
CHEMBL3660645 1 10.25
CHEMBL3906366 1 10.01
CHEMBL3660642 1 9.88
CHEMBL3660646 1 9.77
CHEMBL3660640 1 9.72
CHEMBL3660643 1 9.43
CHEMBL3660641 1 9.30
CHEMBL3656315 1 9.01
CHEMBL3660579 1 9.00
CHEMBL3660632 1 9.00
CHEMBL3660637 1 8.95
CHEMBL3660639 1 8.94
CHEMBL3660586 1 8.85
CHEMBL3660499 1 8.78
CHEMBL3660585 1 8.70
CHEMBL3660605 1 8.70
CHEMBL3660623 1 8.70
CHEMBL3660634 1 8.70
CHEMBL3660638 1 8.69
CHEMBL3660636 1 8.64
CHEMBL3660635 1 8.63
CHEMBL3660581 1 8.52
CHEMBL3660584 1 8.52
CHEMBL3660622 1 8.52
CHEMBL3660593 1 8.47
CHEMBL3660607 1 8.41
CHEMBL3660553 1 8.31

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3660647 IC50 = 0.04 nM 10.40
CHEMBL2180802 IC50 = 0.045 nM 10.35
CHEMBL3660644 IC50 = 0.055 nM 10.26
CHEMBL3660645 IC50 = 0.056 nM 10.25
CHEMBL3906366 IC50 = 0.098 nM 10.01
CHEMBL3660642 IC50 = 0.132 nM 9.88
CHEMBL3660646 IC50 = 0.171 nM 9.77
CHEMBL3660640 IC50 = 0.189 nM 9.72
CHEMBL3660643 IC50 = 0.369 nM 9.43
CHEMBL3660641 IC50 = 0.502 nM 9.30
CHEMBL3656315 IC50 = 0.97 nM 9.01
CHEMBL3660632 IC50 = 1.0 nM 9.00
CHEMBL3660579 IC50 = 1.0 nM 9.00
CHEMBL3660637 IC50 = 1.134 nM 8.95
CHEMBL3660639 IC50 = 1.148 nM 8.94
CHEMBL3660586 IC50 = 1.422 nM 8.85
CHEMBL3660499 IC50 = 1.661 nM 8.78
CHEMBL3660647 IC50 = 2.0 nM 8.70
CHEMBL3660634 IC50 = 2.0 nM 8.70
CHEMBL3660623 IC50 = 2.0 nM 8.70
CHEMBL3660605 IC50 = 2.0 nM 8.70
CHEMBL3660585 IC50 = 2.0 nM 8.70
CHEMBL3660638 IC50 = 2.064 nM 8.69
CHEMBL3660636 IC50 = 2.298 nM 8.64
CHEMBL3660635 IC50 = 2.319 nM 8.63
CHEMBL3660647 IC50 = 3.0 nM 8.52
CHEMBL3660581 IC50 = 3.0 nM 8.52
CHEMBL3660622 IC50 = 3.0 nM 8.52
CHEMBL3660584 IC50 = 3.0 nM 8.52
CHEMBL3660593 IC50 = 3.418 nM 8.47
CHEMBL3660607 IC50 = 3.9 nM 8.41
CHEMBL3660553 IC50 = 4.944 nM 8.31
CHEMBL3660633 IC50 = 5.0 nM 8.30
CHEMBL3660602 IC50 = 5.0 nM 8.30
CHEMBL3660583 IC50 = 5.0 nM 8.30
CHEMBL3660564 IC50 = 5.012 nM 8.30
CHEMBL3660504 IC50 = 5.25 nM 8.28
CHEMBL3660546 IC50 = 5.39 nM 8.27
CHEMBL3660560 IC50 = 5.914 nM 8.23
CHEMBL3660620 IC50 = 6.435 nM 8.19
CHEMBL3660609 IC50 = 7.0 nM 8.15
CHEMBL3660603 IC50 = 7.0 nM 8.15
CHEMBL3660538 IC50 = 7.0 nM 8.15
CHEMBL3660547 IC50 = 7.393 nM 8.13
CHEMBL3660551 IC50 = 7.529 nM 8.12
CHEMBL3660603 IC50 = 8.0 nM 8.10
CHEMBL3639594 IC50 = 8.0 nM 8.10
CHEMBL3660580 IC50 = 8.0 nM 8.10
CHEMBL3660554 IC50 = 8.696 nM 8.06
CHEMBL3660582 IC50 = 9.0 nM 8.05