Skip to main content
Free research Free research Free assay review with research home and workspace preview
Quick search ChEMBL 36
Assay Detail

CHEMBL3706189

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibitory Assay: This test is based on measuring the expression of the AKT protein phosphorylated on serine 473 (P-AKT-S473), in the PC3 human prostate carcinoma line, by means of the technique based on a sandwich immunoassay using the MSD Multi-spot Biomarker Detection kit from Meso Scale Discovery: phospho-Akt (Ser473) whole cell lysate kit (#K151CAD) or phospho-Akt (Ser473)/Total Akt whole cell lysate kit (#K15100D). The primary antibody specific for P-AKT-S473 (Kit #K151CAD) is coated on to an electrode in each well of the 96-well plates of the MSD, kit: after the addition of a protein lysate to each well, the signal is visualised by adding a secondary detection antibody labelled with an electrochemoluminescent compound. The procedure followed is that described in the kit.On day 1, the PC3 cells are seeded into 96-well plates (TPP, #92096) at the concentration of 35 000 cells/well in 200 ul of DMEM medium (DMEM Gibco #11960-044) containing 10% of foetal calf serum (FCS Gibco, #10500-056).
106
Total Activities
106
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type PC-3
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

RAC-alpha serine/threonine-protein kinase (CHEMBL4282)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

(6-oxo-1,6-dihydropyrimidin-2-yl)amide derivatives, preparation thereof and pharmaceutical use thereof as AKT(PKB) phosphorylation inhibitors
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 106 7.15 9.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3112850 1 9.00
CHEMBL3112849 1 8.52
CHEMBL3112851 1 8.52
CHEMBL3699804 1 8.40
CHEMBL3112848 1 8.30
CHEMBL3112862 1 8.22
CHEMBL3112847 1 8.15
CHEMBL3696287 1 8.00
CHEMBL3699780 1 8.00
CHEMBL3696300 1 7.96
CHEMBL3699783 1 7.96
CHEMBL3112867 1 7.92
CHEMBL3112864 1 7.89
CHEMBL3696296 1 7.85
CHEMBL3696307 1 7.82
CHEMBL3699788 1 7.80
CHEMBL3696293 1 7.77
CHEMBL3112866 SAR-260301 1.0 1 7.72
CHEMBL3112861 1 7.70
CHEMBL3699800 1 7.66
CHEMBL3696237 1 7.64
CHEMBL3696314 1 7.64
CHEMBL3696309 1 7.62
CHEMBL3696294 1 7.58
CHEMBL3699779 1 7.58
CHEMBL3699796 1 7.58
CHEMBL3696308 1 7.57
CHEMBL3112865 1 7.55
CHEMBL3699808 1 7.54
CHEMBL3696301 1 7.46

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3112850 IC50 = 1.0 nM 9.00
CHEMBL3112851 IC50 = 3.0 nM 8.52
CHEMBL3112849 IC50 = 3.0 nM 8.52
CHEMBL3699804 IC50 = 4.0 nM 8.40
CHEMBL3112848 IC50 = 5.0 nM 8.30
CHEMBL3112862 IC50 = 6.0 nM 8.22
CHEMBL3112847 IC50 = 7.0 nM 8.15
CHEMBL3699780 IC50 = 10.0 nM 8.00
CHEMBL3696287 IC50 = 10.0 nM 8.00
CHEMBL3699783 IC50 = 11.0 nM 7.96
CHEMBL3696300 IC50 = 11.0 nM 7.96
CHEMBL3112867 IC50 = 12.0 nM 7.92
CHEMBL3112864 IC50 = 13.0 nM 7.89
CHEMBL3696296 IC50 = 14.0 nM 7.85
CHEMBL3696307 IC50 = 15.0 nM 7.82
CHEMBL3699788 IC50 = 16.0 nM 7.80
CHEMBL3696293 IC50 = 17.0 nM 7.77
CHEMBL3112866 SAR-260301 IC50 = 19.0 nM 7.72
CHEMBL3112861 IC50 = 20.0 nM 7.70
CHEMBL3699800 IC50 = 22.0 nM 7.66
CHEMBL3696237 IC50 = 23.0 nM 7.64
CHEMBL3696314 IC50 = 23.0 nM 7.64
CHEMBL3696309 IC50 = 24.0 nM 7.62
CHEMBL3696294 IC50 = 26.0 nM 7.58
CHEMBL3699796 IC50 = 26.0 nM 7.58
CHEMBL3699779 IC50 = 26.0 nM 7.58
CHEMBL3696308 IC50 = 27.0 nM 7.57
CHEMBL3112865 IC50 = 28.0 nM 7.55
CHEMBL3699808 IC50 = 29.0 nM 7.54
CHEMBL3699797 IC50 = 35.0 nM 7.46
CHEMBL3696301 IC50 = 35.0 nM 7.46
CHEMBL3639986 IC50 = 38.0 nM 7.42
CHEMBL3699793 IC50 = 41.0 nM 7.39
CHEMBL3696241 IC50 = 42.0 nM 7.38
CHEMBL3696306 IC50 = 42.0 nM 7.38
CHEMBL3696311 IC50 = 43.0 nM 7.37
CHEMBL3699806 IC50 = 43.0 nM 7.37
CHEMBL3696305 IC50 = 43.0 nM 7.37
CHEMBL3699784 IC50 = 44.0 nM 7.36
CHEMBL3699810 IC50 = 49.0 nM 7.31
CHEMBL3696274 IC50 = 50.0 nM 7.30
CHEMBL3696236 IC50 = 51.0 nM 7.29
CHEMBL3699781 IC50 = 51.0 nM 7.29
CHEMBL3696310 IC50 = 56.0 nM 7.25
CHEMBL3699811 IC50 = 57.0 nM 7.24
CHEMBL3696298 IC50 = 57.0 nM 7.24
CHEMBL3696249 IC50 = 58.0 nM 7.24
CHEMBL3112852 IC50 = 60.0 nM 7.22
CHEMBL3696258 IC50 = 60.0 nM 7.22
CHEMBL3699789 IC50 = 61.0 nM 7.21