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Assay Detail

CHEMBL3887326

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
CYP3A4 Inhibition Assay: The CYP3A4 inhibition assay was performed using human liver microsomes and testosterone 6'-hydroxylation as a P450 isoform-specific marker. In a total volume of 150 uL, 14C-testosterone at a final concentration of 40 uM in a 100 mM phosphate buffer (pH 7.4) was incubated in a 96-well plate with 0.3 mg/mL of human liver microsomes in an Eppendorf thermomixer at 37° C. and 400 rpm. A 1.0 uL-aliquot of the 150-fold concentrated compound stock solution, prepared in DMSO, was added to yield final inhibitor concentrations of 0, 0.1, 0.5, 1.0, 5.0, 10, 25, and 50 uM. The reaction was initiated by addition of 15 uL of the NADPH-regenerating system containing the glucose-6-phosphate dehydrogenase and terminated after 7 min with a 75 uL-aliquot of methanol. After centrifugation at 465 g and 4° C. for 20 min, a 50 uL-aliquot of the supernatant was submitted to HPLC according to the method described below.
165
Total Activities
165
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Tissue Liver
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Cytochrome P450 3A4 (CHEMBL340)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

2-(1,2,3-triazol-2-yl)benzamide and 3-(1,2,3-triazol-2-YL)picolinamide derivatives as orexin receptor antagonists
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 165 4.74 6.52

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3967139 1 6.52
CHEMBL3907374 1 6.22
CHEMBL3920320 1 5.92
CHEMBL3941085 1 5.92
CHEMBL3967251 1 5.70
CHEMBL3912376 1 5.50
CHEMBL3917550 1 5.48
CHEMBL3956147 1 5.29
CHEMBL3905808 1 5.26
CHEMBL3933744 1 5.22
CHEMBL3950355 1 5.22
CHEMBL3905303 1 5.21
CHEMBL3909876 1 5.17
CHEMBL3961204 1 5.13
CHEMBL3959470 1 5.12
CHEMBL3981385 1 5.11
CHEMBL3946411 1 5.08
CHEMBL3957175 1 5.07
CHEMBL3977273 1 5.04
CHEMBL3909380 1 5.04
CHEMBL3926167 1 5.02
CHEMBL3953726 1 5.02
CHEMBL3956556 1 5.02
CHEMBL3910117 1 5.01
CHEMBL3915416 1 5.01
CHEMBL3942007 1 5.01
CHEMBL3943141 1 4.96
CHEMBL3976034 1 4.89
CHEMBL3901878 1 4.89
CHEMBL3933736 1 4.89

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3967139 IC50 = 300.0 nM 6.52
CHEMBL3907374 IC50 = 600.0 nM 6.22
CHEMBL3941085 IC50 = 1200.0 nM 5.92
CHEMBL3920320 IC50 = 1200.0 nM 5.92
CHEMBL3967251 IC50 = 2000.0 nM 5.70
CHEMBL3912376 IC50 = 3200.0 nM 5.50
CHEMBL3917550 IC50 = 3300.0 nM 5.48
CHEMBL3956147 IC50 = 5100.0 nM 5.29
CHEMBL3905808 IC50 = 5500.0 nM 5.26
CHEMBL3933744 IC50 = 6000.0 nM 5.22
CHEMBL3950355 IC50 = 6000.0 nM 5.22
CHEMBL3905303 IC50 = 6100.0 nM 5.21
CHEMBL3909876 IC50 = 6800.0 nM 5.17
CHEMBL3961204 IC50 = 7400.0 nM 5.13
CHEMBL3959470 IC50 = 7500.0 nM 5.12
CHEMBL3981385 IC50 = 7700.0 nM 5.11
CHEMBL3946411 IC50 = 8400.0 nM 5.08
CHEMBL3957175 IC50 = 8500.0 nM 5.07
CHEMBL3909380 IC50 = 9100.0 nM 5.04
CHEMBL3977273 IC50 = 9200.0 nM 5.04
CHEMBL3956556 IC50 = 9600.0 nM 5.02
CHEMBL3953726 IC50 = 9600.0 nM 5.02
CHEMBL3926167 IC50 = 9600.0 nM 5.02
CHEMBL3910117 IC50 = 9700.0 nM 5.01
CHEMBL3942007 IC50 = 9800.0 nM 5.01
CHEMBL3915416 IC50 = 9700.0 nM 5.01
CHEMBL3943141 IC50 = 11000.0 nM 4.96
CHEMBL3901878 IC50 = 13000.0 nM 4.89
CHEMBL3897210 IC50 = 13000.0 nM 4.89
CHEMBL3933736 IC50 = 13000.0 nM 4.89
CHEMBL3976034 IC50 = 13000.0 nM 4.89
CHEMBL3910447 IC50 = 14000.0 nM 4.85
CHEMBL3931693 IC50 = 14000.0 nM 4.85
CHEMBL3923356 IC50 = 14000.0 nM 4.85
CHEMBL3922678 IC50 = 14000.0 nM 4.85
CHEMBL3936704 IC50 = 14000.0 nM 4.85
CHEMBL3982996 IC50 = 14000.0 nM 4.85
CHEMBL3938872 IC50 = 14000.0 nM 4.85
CHEMBL3974746 IC50 = 14000.0 nM 4.85
CHEMBL3938822 IC50 = 15000.0 nM 4.82
CHEMBL3925326 IC50 = 15000.0 nM 4.82
CHEMBL3915231 IC50 = 15000.0 nM 4.82
CHEMBL3946888 IC50 = 16000.0 nM 4.80
CHEMBL3950474 IC50 = 17000.0 nM 4.77
CHEMBL3901849 IC50 = 17000.0 nM 4.77
CHEMBL3914317 IC50 = 17000.0 nM 4.77
CHEMBL3947667 IC50 = 17000.0 nM 4.77
CHEMBL3952666 IC50 = 17000.0 nM 4.77
CHEMBL3901217 IC50 = 17000.0 nM 4.77
CHEMBL3923760 IC50 = 17000.0 nM 4.77