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Assay Detail

CHEMBL3887660

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Shift AlphaScreen Assay : The AlphaScreen Assay is modified to include the testing of inhibitors against ADAMTS-5 in the presence of 50% Lewis rat plasma in order to determine the effects of plasma protein binding on inhibitor potency. The ratio between the IC50 of the inhibitor against ADAMTS-5 in 50% Lewis rat plasma versus the IC50 of the inhibitor in buffer is calculated and is described as the plasma shift of the inhibitor. The assay is completed in the same manner using 10 nM ADAMTS-5 instead of 2.1 nM. A similar assay is used with dog ADAMTS-4 in the presence of 25% dog plasma.
5
Total Activities
5
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Tissue Plasma
Confidence 8 — Homologous single protein target
Curated By Autocuration

Publication

Aggrecanase inhibitors
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 5 7.46 7.82

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4066965 1 7.82
CHEMBL3980860 1 7.75
CHEMBL4072836 1 7.70
CHEMBL3972836 1 7.19
CHEMBL3955404 1 6.84

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4066965 IC50 = 15.0 nM 7.82
CHEMBL3980860 IC50 = 18.0 nM 7.75
CHEMBL4072836 IC50 = 20.0 nM 7.70
CHEMBL3972836 IC50 = 64.0 nM 7.19
CHEMBL3955404 IC50 = 146.0 nM 6.84