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Assay Detail

CHEMBL3889185

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Binding
In Vitro Assay: The effectiveness of compounds of the present invention as ROCK inhibitors can be determined in a 30 μL assay containing 20 mM HEPES, pH 7.5, 20 mM MgCl2, 0.015% Brij-35, 4 mM DTT, 5 μM ATP and 1.5 μM peptide substrate (FITC-AHA-AKRRRLSSLRA-OH). Compounds were dissolved in DMSO so that the final concentration of DMSO was <2%, and the reaction was initiated with Rho kinase variants. After incubation, the reaction was terminated by the addition of EDTA and the phosphorylated and non-phosphorylated peptides separated using a LABCHIP® 3000 Reader (Caliper Life Sciences). Controls consisted of assays that did not contain compound, and backgrounds consisted of assays that contained enzyme and substrate but had EDTA from the beginning of the reaction to inhibit kinase activity.
316
Total Activities
285
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Rho-associated protein kinase 1 (CHEMBL3231)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Phenylpyrazole derivatives as potent ROCK1 and ROCK2 inhibitors
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 316 7.37 9.70

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4107027 1 9.70
CHEMBL3902471 1 9.59
CHEMBL3961538 1 9.41
CHEMBL3949136 1 9.37
CHEMBL4114628 1 9.11
CHEMBL3986802 1 9.07
CHEMBL3964418 1 8.98
CHEMBL3913336 1 8.96
CHEMBL3925017 1 8.91
CHEMBL3901295 3 8.81
CHEMBL3957651 1 8.81
CHEMBL3910152 1 8.75
CHEMBL4115244 1 8.67
CHEMBL4113669 1 8.65
CHEMBL4107997 1 8.65
CHEMBL3956238 1 8.62
CHEMBL3947008 1 8.61
CHEMBL4107343 1 8.61
CHEMBL3928809 1 8.58
CHEMBL3958305 1 8.52
CHEMBL3965274 3 8.51
CHEMBL3920062 1 8.50
CHEMBL3904054 1 8.49
CHEMBL3961024 1 8.49
CHEMBL3969934 1 8.47
CHEMBL3898965 2 8.47
CHEMBL3977577 1 8.47
CHEMBL4107839 1 8.47
CHEMBL3939581 1 8.38
CHEMBL3960736 1 8.37

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4107027 IC50 = 0.2 nM 9.70
CHEMBL3902471 IC50 = 0.26 nM 9.59
CHEMBL3961538 IC50 = 0.39 nM 9.41
CHEMBL3949136 IC50 = 0.43 nM 9.37
CHEMBL4114628 IC50 = 0.77 nM 9.11
CHEMBL3986802 IC50 = 0.85 nM 9.07
CHEMBL3964418 IC50 = 1.04 nM 8.98
CHEMBL3913336 IC50 = 1.11 nM 8.96
CHEMBL3925017 IC50 = 1.24 nM 8.91
CHEMBL3901295 IC50 = 1.53 nM 8.81
CHEMBL3957651 IC50 = 1.54 nM 8.81
CHEMBL3910152 IC50 = 1.79 nM 8.75
CHEMBL4115244 IC50 = 2.15 nM 8.67
CHEMBL4113669 IC50 = 2.22 nM 8.65
CHEMBL4107997 IC50 = 2.26 nM 8.65
CHEMBL3956238 IC50 = 2.39 nM 8.62
CHEMBL3947008 IC50 = 2.44 nM 8.61
CHEMBL4107343 IC50 = 2.46 nM 8.61
CHEMBL3928809 IC50 = 2.63 nM 8.58
CHEMBL3958305 IC50 = 3.05 nM 8.52
CHEMBL3965274 IC50 = 3.1 nM 8.51
CHEMBL3920062 IC50 = 3.16 nM 8.50
CHEMBL3965274 IC50 = 3.17 nM 8.50
CHEMBL3904054 IC50 = 3.26 nM 8.49
CHEMBL3961024 IC50 = 3.24 nM 8.49
CHEMBL3898965 IC50 = 3.36 nM 8.47
CHEMBL4107839 IC50 = 3.38 nM 8.47
CHEMBL3969934 IC50 = 3.37 nM 8.47
CHEMBL3977577 IC50 = 3.38 nM 8.47
CHEMBL3939581 IC50 = 4.22 nM 8.38
CHEMBL3960736 IC50 = 4.27 nM 8.37
CHEMBL3939886 IC50 = 4.25 nM 8.37
CHEMBL4110459 IC50 = 4.62 nM 8.34
CHEMBL3956875 IC50 = 4.6 nM 8.34
CHEMBL3901295 IC50 = 4.7 nM 8.33
CHEMBL3907133 IC50 = 5.35 nM 8.27
CHEMBL3946084 IC50 = 5.5 nM 8.26
CHEMBL3915532 IC50 = 5.77 nM 8.24
CHEMBL3936323 IC50 = 5.91 nM 8.23
CHEMBL4111518 IC50 = 5.98 nM 8.22
CHEMBL4109081 IC50 = 6.45 nM 8.19
CHEMBL3955270 IC50 = 6.39 nM 8.19
CHEMBL3928198 IC50 = 6.53 nM 8.19
CHEMBL3951271 IC50 = 6.69 nM 8.18
CHEMBL4107374 IC50 = 6.62 nM 8.18
CHEMBL3969951 IC50 = 6.68 nM 8.18
CHEMBL4108559 IC50 = 6.55 nM 8.18
CHEMBL4114533 IC50 = 7.09 nM 8.15
CHEMBL4112558 IC50 = 7.0 nM 8.15
CHEMBL3947211 IC50 = 7.22 nM 8.14