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Assay Detail

CHEMBL4425316

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of human His-tagged PDE4B catalytic domain expressed in Escherichia coli BL21-CodonPlus(DE3) cells using [3H]cAMP or [3H]cGMP as substrate incubated for 30 mins by scintillation counting method
11
Total Activities
11
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

3',5'-cyclic-AMP phosphodiesterase 4B (CHEMBL275)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

PDEStrIAn: A Phosphodiesterase Structure and Ligand Interaction Annotated Database As a Tool for Structure-Based Drug Design.
Jansen C, Kooistra AJ, Kanev GK, Leurs R, de Esch IJ, de Graaf C.
J Med Chem (2016) 59 : 7029 -7065
PubMed 26908025 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 11 6.84 10.39

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL42126 PICLAMILAST 2.0 1 10.39
CHEMBL511115 CILOMILAST 3.0 1 7.60
CHEMBL1230564 1 7.48
CHEMBL519827 1 7.25
CHEMBL193240 ROFLUMILAST 4.0 1 7.08
CHEMBL430893 (-)-ROLIPRAM 1 6.64
CHEMBL603830 DAXALIPRAM 2.0 1 6.38
CHEMBL63 ROLIPRAM 2.0 1 6.26
CHEMBL590754 FILAMINAST 2.0 1 6.02
CHEMBL168949 1 5.42
CHEMBL192 SILDENAFIL 4.0 1 4.70

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL42126 PICLAMILAST IC50 = 0.041 nM 10.39
CHEMBL511115 CILOMILAST IC50 = 25.0 nM 7.60
CHEMBL1230564 IC50 = 33.0 nM 7.48
CHEMBL519827 IC50 = 56.0 nM 7.25
CHEMBL193240 ROFLUMILAST IC50 = 84.0 nM 7.08
CHEMBL430893 (-)-ROLIPRAM IC50 = 231.0 nM 6.64
CHEMBL603830 DAXALIPRAM IC50 = 420.0 nM 6.38
CHEMBL63 ROLIPRAM IC50 = 550.0 nM 6.26
CHEMBL590754 FILAMINAST IC50 = 960.0 nM 6.02
CHEMBL168949 IC50 = 3800.0 nM 5.42
CHEMBL192 SILDENAFIL IC50 = 20000.0 nM 4.70