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Assay Detail

CHEMBL4680700

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of human full length FLAG-tagged PRMT5/human His6-tagged MEP50 expressed in baculovirus-infected Sf9 cells assessed as reduction in tritium incorporation into peptide substrate using human Histone H4 (1 to 15 residues) and [3H]SAM as substrate preincubated with enzyme and H4 for 30 mins followed by [3H]SAM addition and measured after 120 mins by radioactive flashplate assay
16
Total Activities
16
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type Sf9
Confidence 7 — Homologous single protein target
Curated By Autocuration

Target

PRMT5/MEP50 complex (CHEMBL3137261)
Type PROTEIN COMPLEX
Organism Homo sapiens

Publication

Structure and Property Guided Design in the Identification of PRMT5 Tool Compound EPZ015666.
Duncan KW,Rioux N,Boriack-Sjodin PA,Munchhof MJ,Reiter LA,Majer CR,Jin L,Johnston LD,Chan-Penebre E,Kuplast KG,Porter Scott M,Pollock RM,Waters NJ,Smith JJ,Moyer MP,Copeland RA,Chesworth R
ACS Med Chem Lett (2016) 7 : 162 -166
PubMed 26985292 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 16 7.13 8.40

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4542380 1 8.40
CHEMBL3958947 1 7.96
CHEMBL3963350 1 7.89
CHEMBL3927051 1 7.89
CHEMBL3938760 1 7.75
CHEMBL4060831 1 7.66
CHEMBL3919677 1 7.64
CHEMBL3913586 1 7.48
CHEMBL3977219 1 7.14
CHEMBL3914119 1 7.02
CHEMBL3962874 1 6.84
CHEMBL3890510 1 6.49
CHEMBL3906136 1 5.13
CHEMBL4754920 1 4.57
CHEMBL3982868 1 -
CHEMBL4764863 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4542380 IC50 = 4.0 nM 8.40
CHEMBL3958947 IC50 = 11.0 nM 7.96
CHEMBL3963350 IC50 = 13.0 nM 7.89
CHEMBL3927051 IC50 = 13.0 nM 7.89
CHEMBL3938760 IC50 = 18.0 nM 7.75
CHEMBL4060831 IC50 = 22.0 nM 7.66
CHEMBL3919677 IC50 = 23.0 nM 7.64
CHEMBL3913586 IC50 = 33.0 nM 7.48
CHEMBL3977219 IC50 = 73.0 nM 7.14
CHEMBL3914119 IC50 = 95.0 nM 7.02
CHEMBL3962874 IC50 = 144.0 nM 6.84
CHEMBL3890510 IC50 = 326.0 nM 6.49
CHEMBL3906136 IC50 = 7450.0 nM 5.13
CHEMBL4754920 IC50 = 26800.0 nM 4.57
CHEMBL3982868 IC50 > 50000.0 nM -
CHEMBL4764863 IC50 > 50000.0 nM -