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Assay Detail

CHEMBL5732962

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Kinase Inhibition Assay: Kinase inhibition can be determined using an IMAP® assay (Molecular Devices). This assay method involves the use of a fluorescently-tagged peptide substrate. Phosphorylation of the tagged peptide by a kinase of interest promotes binding of the peptide to a trivalent metal-based nanoparticle via the specific, high affinity interaction between the phospho-group and the trivalent metal. Proximity to the nanoparticle results in increased fluorescence polarization Inhibition of the kinase by a kinase inhibitor prevents phosphorylation of the substrate and thereby limits binding of the fluorescently-tagged substrate to the nanoparticle. Such an assay can be compatible with a microwell assay format, allowing simultaneous determination of IC50 of multiple compounds.
42
Total Activities
6
Compounds Tested
4
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Rho-associated protein kinase 1 (CHEMBL3231)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Rho kinase inhibitors
(2017)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
kon 14 - -
k_off 14 - -
IC50 7 5.31 6.48
Ki 7 6.74 8.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5768727 6 8.00
CHEMBL5850670 6 7.40
CHEMBL5858473 12 7.16
CHEMBL6016872 6 6.58
CHEMBL2005186 BELUMOSUDIL 4.0 6 6.30
CHEMBL5850835 6 5.70

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5768727 Ki = 10.0 nM 8.00
CHEMBL5850670 Ki = 40.0 nM 7.40
CHEMBL5858473 Ki = 70.0 nM 7.16
CHEMBL6016872 Ki = 260.0 nM 6.58
CHEMBL5768727 IC50 = 330.0 nM 6.48
CHEMBL2005186 BELUMOSUDIL Ki = 500.0 nM 6.30
CHEMBL5858473 Ki = 870.0 nM 6.06
CHEMBL5850670 IC50 = 1130.0 nM 5.95
CHEMBL5858473 IC50 = 1770.0 nM 5.75
CHEMBL5850835 Ki = 2010.0 nM 5.70
CHEMBL6016872 IC50 = 6690.0 nM 5.17
CHEMBL2005186 BELUMOSUDIL IC50 = 13110.0 nM 4.88
CHEMBL5858473 IC50 = 22530.0 nM 4.65
CHEMBL5850835 IC50 = 53450.0 nM 4.27
CHEMBL5858473 kon = - -
CHEMBL5858473 k_off = - s-1 -
CHEMBL5850835 kon = - -
CHEMBL5850835 k_off = - s-1 -
CHEMBL5850835 kon = - -
CHEMBL5850835 k_off = - s-1 -
CHEMBL5850670 kon = - -
CHEMBL6016872 k_off = - s-1 -
CHEMBL6016872 kon = - -
CHEMBL6016872 k_off = - s-1 -
CHEMBL2005186 BELUMOSUDIL kon = - -
CHEMBL2005186 BELUMOSUDIL k_off = - s-1 -
CHEMBL2005186 BELUMOSUDIL kon = - -
CHEMBL2005186 BELUMOSUDIL k_off = - s-1 -
CHEMBL5858473 k_off = - s-1 -
CHEMBL5858473 kon = - -
CHEMBL6016872 kon = - -
CHEMBL5858473 k_off = - s-1 -
CHEMBL5850670 k_off = - s-1 -
CHEMBL5858473 kon = - -
CHEMBL5858473 k_off = - s-1 -
CHEMBL5850670 kon = - -
CHEMBL5850670 k_off = - s-1 -
CHEMBL5768727 kon = - -
CHEMBL5858473 kon = - -
CHEMBL5768727 k_off = - s-1 -
CHEMBL5768727 kon = - -
CHEMBL5768727 k_off = - s-1 -