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Assay Detail

CHEMBL3705582

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Binding
Inhibition Assay: When setting conditions for the measurement of the inhibitory effect of the compounds on FGFR2 kinase activity, FL-Peptide 22 (Caliper Life Sciences, Inc.) was used as a substrate. The purified recombinant human FGFR2 protein used in the test was purchased from Carna Biosciences, Inc. In the measurement of the inhibitory effect of the compounds, first, a test compound was gradually diluted with dimethylsulfoxide (DMSO) to a concentration that was 20 times higher than the final concentration. Next, the purified human FGFR2 protein, FL-Peptide 22 (final concentration: 1.5 .mu.M), magnesium chloride (final concentration: 5 mM), ATP (final concentration: 75 .mu.M), and the test compound DMSO solution (final concentration of DMSO: 5%) were added to a reaction buffer (15 mM Tris-HCl pH 7.5, 0.01% Tween-20, 2 mM DTT), and the mixture was incubated at 25.degree. C. for 120 minutes to perform a kinase reaction. EDTA (final concentration: 30 mM) diluted with a separation buffer.
52
Total Activities
50
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Fibroblast growth factor receptor 2 (CHEMBL4142)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

3,5-disubstituted alkynylbenzene compound and salt thereof
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 52 8.32 9.40

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3701256 1 9.40
CHEMBL3701258 2 9.40
CHEMBL3701268 1 9.22
CHEMBL3701275 1 9.00
CHEMBL3701267 2 9.00
CHEMBL3701238 FUTIBATINIB 4.0 1 8.96
CHEMBL3701239 1 8.96
CHEMBL3701241 1 8.96
CHEMBL3701279 1 8.92
CHEMBL3701242 1 8.92
CHEMBL3701271 1 8.92
CHEMBL3701272 1 8.82
CHEMBL3701270 1 8.82
CHEMBL3701262 1 8.70
CHEMBL3701243 1 8.66
CHEMBL3701273 1 8.64
CHEMBL3701237 1 8.62
CHEMBL3701269 1 8.60
CHEMBL3701249 1 8.57
CHEMBL3701245 1 8.52
CHEMBL3701259 1 8.49
CHEMBL3701250 1 8.48
CHEMBL3701254 1 8.43
CHEMBL3701244 1 8.42
CHEMBL3701246 1 8.42
CHEMBL3701247 1 8.39
CHEMBL3701261 1 8.37
CHEMBL3701248 1 8.37
CHEMBL3701257 1 8.33
CHEMBL3701251 1 8.25

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3701256 IC50 = 0.4 nM 9.40
CHEMBL3701258 IC50 = 0.4 nM 9.40
CHEMBL3701268 IC50 = 0.6 nM 9.22
CHEMBL3701267 IC50 = 1.0 nM 9.00
CHEMBL3701275 IC50 = 1.0 nM 9.00
CHEMBL3701238 FUTIBATINIB IC50 = 1.1 nM 8.96
CHEMBL3701239 IC50 = 1.1 nM 8.96
CHEMBL3701241 IC50 = 1.1 nM 8.96
CHEMBL3701242 IC50 = 1.2 nM 8.92
CHEMBL3701271 IC50 = 1.2 nM 8.92
CHEMBL3701279 IC50 = 1.2 nM 8.92
CHEMBL3701272 IC50 = 1.5 nM 8.82
CHEMBL3701267 IC50 = 1.5 nM 8.82
CHEMBL3701270 IC50 = 1.5 nM 8.82
CHEMBL3701262 IC50 = 2.0 nM 8.70
CHEMBL3701243 IC50 = 2.2 nM 8.66
CHEMBL3701273 IC50 = 2.3 nM 8.64
CHEMBL3701237 IC50 = 2.4 nM 8.62
CHEMBL3701269 IC50 = 2.5 nM 8.60
CHEMBL3701249 IC50 = 2.7 nM 8.57
CHEMBL3701245 IC50 = 3.0 nM 8.52
CHEMBL3701259 IC50 = 3.2 nM 8.49
CHEMBL3701250 IC50 = 3.3 nM 8.48
CHEMBL3701254 IC50 = 3.7 nM 8.43
CHEMBL3701246 IC50 = 3.8 nM 8.42
CHEMBL3701244 IC50 = 3.8 nM 8.42
CHEMBL3701247 IC50 = 4.1 nM 8.39
CHEMBL3701261 IC50 = 4.3 nM 8.37
CHEMBL3701248 IC50 = 4.3 nM 8.37
CHEMBL3701257 IC50 = 4.7 nM 8.33
CHEMBL3701258 IC50 = 4.9 nM 8.31
CHEMBL3701251 IC50 = 5.6 nM 8.25
CHEMBL3701265 IC50 = 5.8 nM 8.24
CHEMBL3701260 IC50 = 6.6 nM 8.18
CHEMBL3701263 IC50 = 6.8 nM 8.17
CHEMBL3701252 IC50 = 6.8 nM 8.17
CHEMBL3701240 IC50 = 6.9 nM 8.16
CHEMBL3701264 IC50 = 7.0 nM 8.15
CHEMBL3701277 IC50 = 7.0 nM 8.15
CHEMBL3701253 IC50 = 7.2 nM 8.14
CHEMBL3701276 IC50 = 7.9 nM 8.10
CHEMBL3701280 IC50 = 8.8 nM 8.06
CHEMBL3701255 IC50 = 9.3 nM 8.03
CHEMBL3701285 IC50 = 110.0 nM 6.96
CHEMBL3701282 IC50 = 190.0 nM 6.72
CHEMBL3701284 IC50 = 190.0 nM 6.72
CHEMBL3701281 IC50 = 270.0 nM 6.57
CHEMBL1873475 IBRUTINIB IC50 = 280.0 nM 6.55
CHEMBL3701286 IC50 = 1600.0 nM 5.80
CHEMBL3701278 IC50 < 0.3 nM -