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Assay Detail

CHEMBL3706019

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Binding Assay: Human recombinant PDE4 (Gene bank accession no NM006203) was incubated for 1 hour with the test compound at concentrations up to 10 μM, with cAMP (1x10-5M), and with a low amount (0.021 MBq) of radioactively labelled cAMP. At the end of the incubation, the cleavage of the substrate was evaluated by the binding of the AMP product to SPA beads, which generate chemo luminescence when bound to the radioactive tracer. The AMP product inhibited the binding of the radioactive tracer to the beads, and the luminescent signal was competed.
28
Total Activities
28
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

3',5'-cyclic-AMP phosphodiesterase 4A (CHEMBL254)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Triazolopyridines as phosphodiesterase inhibitors for treatment of dermal diseases
(2014)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 28 7.88 10.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3676245 1 10.00
CHEMBL3676246 1 9.70
CHEMBL3676244 1 9.70
CHEMBL3639751 1 9.52
CHEMBL3676243 1 9.40
CHEMBL3676240 1 9.30
CHEMBL3676242 1 9.15
CHEMBL3676241 1 9.00
CHEMBL3676231 1 8.70
CHEMBL3676257 1 8.52
CHEMBL3676247 1 8.52
CHEMBL3676236 1 8.40
CHEMBL3676233 1 8.15
CHEMBL3676248 1 8.10
CHEMBL3676239 1 7.62
CHEMBL3676234 1 7.58
CHEMBL3676237 1 7.35
CHEMBL3676256 1 7.34
CHEMBL3676253 1 7.28
CHEMBL3676238 1 7.26
CHEMBL3676252 1 7.17
CHEMBL3676232 1 6.87
CHEMBL3676251 1 6.58
CHEMBL3676235 1 6.52
CHEMBL3676255 1 6.26
CHEMBL3676249 1 5.60
CHEMBL3676254 1 5.51
CHEMBL3676250 1 5.44

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3676245 IC50 = 0.1 nM 10.00
CHEMBL3676246 IC50 = 0.2 nM 9.70
CHEMBL3676244 IC50 = 0.2 nM 9.70
CHEMBL3639751 IC50 = 0.3 nM 9.52
CHEMBL3676243 IC50 = 0.4 nM 9.40
CHEMBL3676240 IC50 = 0.5 nM 9.30
CHEMBL3676242 IC50 = 0.7 nM 9.15
CHEMBL3676241 IC50 = 1.0 nM 9.00
CHEMBL3676231 IC50 = 2.0 nM 8.70
CHEMBL3676257 IC50 = 3.0 nM 8.52
CHEMBL3676247 IC50 = 3.0 nM 8.52
CHEMBL3676236 IC50 = 4.0 nM 8.40
CHEMBL3676233 IC50 = 7.0 nM 8.15
CHEMBL3676248 IC50 = 8.0 nM 8.10
CHEMBL3676239 IC50 = 24.0 nM 7.62
CHEMBL3676234 IC50 = 26.0 nM 7.58
CHEMBL3676237 IC50 = 45.0 nM 7.35
CHEMBL3676256 IC50 = 46.0 nM 7.34
CHEMBL3676253 IC50 = 52.0 nM 7.28
CHEMBL3676238 IC50 = 55.0 nM 7.26
CHEMBL3676252 IC50 = 68.0 nM 7.17
CHEMBL3676232 IC50 = 134.0 nM 6.87
CHEMBL3676251 IC50 = 261.0 nM 6.58
CHEMBL3676235 IC50 = 305.0 nM 6.52
CHEMBL3676255 IC50 = 548.0 nM 6.26
CHEMBL3676249 IC50 = 2500.0 nM 5.60
CHEMBL3676254 IC50 = 3100.0 nM 5.51
CHEMBL3676250 IC50 = 3600.0 nM 5.44