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Assay Detail

CHEMBL3887672

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Dopamine D2 Receptor Binding Assay: The assay was performed according to the method by Kohler et al. (Kohler C, Hall H, Ogren S O and Gawell L, Specific in vitro and in vivo binding of 3H-raclopride. A potent substituted benzamide drug with high affinity for dopamine D-2 receptors in the rat brain. Biochem. Pharmacol., 1985; 34: 2251-2259). The binding assay was performed using 40 ul of the membrane specimen, 20 ul of [3H]-raclopride (final concentration 1 to 2 nM), 20 ul of a test drug and 50 mM Tris-hydrochloric acid buffer (containing 120 mM NaCl, 5 mM KCl, 2 mM CaCl2, 1 mM MgCl2, pH 7.4) so that the total amount was 200 ul (final dimethylsulfoxide concentration 1%). The reaction was performed at room temperature for 1 hour and terminated by conducting suction filtration with a cell harvester on a glass fiber filter plate. The filter plate made of glass fiber was washed with 50 mM Tris-hydrochloric acid buffer (pH 7.4), and after dried, a microplate liquid scintillation cocktail was added.
60
Total Activities
59
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Rattus norvegicus
Tissue Brain
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

D(2) dopamine receptor (CHEMBL339)
Type SINGLE PROTEIN
Organism Rattus norvegicus

Publication

Piperazine-substituted benzothiophenes for treatment of mental disorders
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 60 8.88 10.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3907711 2 10.00
CHEMBL2105760 BREXPIPRAZOLE 4.0 1 9.70
CHEMBL3966032 1 9.70
CHEMBL3893296 1 9.70
CHEMBL3901333 1 9.40
CHEMBL3953082 1 9.40
CHEMBL3945539 1 9.30
CHEMBL3974916 1 9.30
CHEMBL3931169 1 9.30
CHEMBL3936629 1 9.22
CHEMBL3962323 1 9.15
CHEMBL3965773 1 9.15
CHEMBL3939353 1 9.15
CHEMBL3899929 1 9.10
CHEMBL3969756 1 9.10
CHEMBL3969404 1 9.10
CHEMBL3905737 1 9.10
CHEMBL3960031 1 9.00
CHEMBL3932669 1 9.00
CHEMBL3942695 1 8.96
CHEMBL3929237 1 8.92
CHEMBL3915465 1 8.92
CHEMBL3905706 1 8.92
CHEMBL3948017 1 8.92
CHEMBL3920216 1 8.92
CHEMBL3941669 1 8.89
CHEMBL3981820 1 8.85
CHEMBL3935871 1 8.85
CHEMBL3985224 1 8.82
CHEMBL3956410 1 8.82

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3907711 Ki = 0.1 nM 10.00
CHEMBL3907711 Ki = 0.1 nM 10.00
CHEMBL3893296 Ki = 0.2 nM 9.70
CHEMBL3966032 Ki = 0.2 nM 9.70
CHEMBL2105760 BREXPIPRAZOLE Ki = 0.2 nM 9.70
CHEMBL3953082 Ki = 0.4 nM 9.40
CHEMBL3901333 Ki = 0.4 nM 9.40
CHEMBL3945539 Ki = 0.5 nM 9.30
CHEMBL3931169 Ki = 0.5 nM 9.30
CHEMBL3974916 Ki = 0.5 nM 9.30
CHEMBL3936629 Ki = 0.6 nM 9.22
CHEMBL3962323 Ki = 0.7 nM 9.15
CHEMBL3939353 Ki = 0.7 nM 9.15
CHEMBL3965773 Ki = 0.7 nM 9.15
CHEMBL3905737 Ki = 0.8 nM 9.10
CHEMBL3969404 Ki = 0.8 nM 9.10
CHEMBL3899929 Ki = 0.8 nM 9.10
CHEMBL3969756 Ki = 0.8 nM 9.10
CHEMBL3960031 Ki = 1.0 nM 9.00
CHEMBL3932669 Ki = 1.0 nM 9.00
CHEMBL3942695 Ki = 1.1 nM 8.96
CHEMBL3920216 Ki = 1.2 nM 8.92
CHEMBL3948017 Ki = 1.2 nM 8.92
CHEMBL3915465 Ki = 1.2 nM 8.92
CHEMBL3929237 Ki = 1.2 nM 8.92
CHEMBL3905706 Ki = 1.2 nM 8.92
CHEMBL3941669 Ki = 1.3 nM 8.89
CHEMBL3981820 Ki = 1.4 nM 8.85
CHEMBL3935871 Ki = 1.4 nM 8.85
CHEMBL3985224 Ki = 1.5 nM 8.82
CHEMBL3956410 Ki = 1.5 nM 8.82
CHEMBL3911283 Ki = 1.5 nM 8.82
CHEMBL3933730 Ki = 1.6 nM 8.80
CHEMBL3937293 Ki = 1.6 nM 8.80
CHEMBL3958333 Ki = 1.7 nM 8.77
CHEMBL3905367 Ki = 1.9 nM 8.72
CHEMBL3977357 Ki = 1.9 nM 8.72
CHEMBL3898190 Ki = 2.0 nM 8.70
CHEMBL3902274 Ki = 2.2 nM 8.66
CHEMBL3979507 Ki = 2.3 nM 8.64
CHEMBL3976061 Ki = 2.3 nM 8.64
CHEMBL3980869 Ki = 2.4 nM 8.62
CHEMBL3889759 Ki = 2.4 nM 8.62
CHEMBL3893739 Ki = 2.6 nM 8.59
CHEMBL3969878 Ki = 2.6 nM 8.59
CHEMBL3909275 Ki = 2.7 nM 8.57
CHEMBL3918214 Ki = 2.8 nM 8.55
CHEMBL3892225 Ki = 3.2 nM 8.49
CHEMBL3890947 Ki = 3.2 nM 8.49
CHEMBL3903749 Ki = 3.3 nM 8.48