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Assay Detail

CHEMBL3887673

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Serotonin 5-HT2A Receptor Binding Assay: The assay was performed according to the method by Leysen J E et al. (Leysen J E, Niemegeers C J E, Van Nueten J M and Laduron P M. [3H] Ketanserin (R 41 468), a selective 3H-ligand for serotonin 2 receptor binding sites. Mol. Pharmacol., 1982, 21: 301-314). The binding assay was performed using 40 ul of the membrane specimen, 20 ul of [3H]-Ketanserin (final concentration 1 to 3 nM), 20 ul of a test drug and 50 mM Tris-hydrochloric acid buffer (pH 7.4) so that the total amount was 200 ul (final dimethylsulfoxide concentration 1%). The reaction was performed at 37° C. for 20 minutes and terminated by conducting suction filtration with a cell harvester on a glass fiber filter plate.The filter plate made of glass fiber was washed with 50 mM Tris-hydrochloric acid buffer (pH 7.4), and after dried, a microplate liquid scintillation cocktail was added and the radioactivity was measured with a microplate scintillation counter.
62
Total Activities
61
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Rattus norvegicus
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

5-hydroxytryptamine receptor 2A (CHEMBL322)
Type SINGLE PROTEIN
Organism Rattus norvegicus

Publication

Piperazine-substituted benzothiophenes for treatment of mental disorders
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 62 8.46 9.22

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3958663 1 9.22
CHEMBL3930364 1 9.00
CHEMBL3915465 1 8.92
CHEMBL3934217 1 8.89
CHEMBL3904588 1 8.89
CHEMBL3982910 1 8.82
CHEMBL3905706 1 8.82
CHEMBL3939353 1 8.77
CHEMBL3965773 1 8.70
CHEMBL3932669 1 8.68
CHEMBL3948017 1 8.68
CHEMBL3933730 1 8.68
CHEMBL3907711 2 8.68
CHEMBL3907815 1 8.64
CHEMBL3945539 1 8.64
CHEMBL2105760 BREXPIPRAZOLE 4.0 1 8.64
CHEMBL3956410 1 8.60
CHEMBL3957163 1 8.59
CHEMBL3969404 1 8.59
CHEMBL3902274 1 8.55
CHEMBL3929237 1 8.55
CHEMBL3902391 1 8.54
CHEMBL3903749 1 8.54
CHEMBL3905737 1 8.54
CHEMBL3901333 1 8.52
CHEMBL3976061 1 8.52
CHEMBL3907222 1 8.51
CHEMBL3905367 1 8.51
CHEMBL3977357 1 8.49
CHEMBL3985224 1 8.48

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3958663 Ki = 0.6 nM 9.22
CHEMBL3930364 Ki = 1.0 nM 9.00
CHEMBL3915465 Ki = 1.2 nM 8.92
CHEMBL3934217 Ki = 1.3 nM 8.89
CHEMBL3904588 Ki = 1.3 nM 8.89
CHEMBL3982910 Ki = 1.5 nM 8.82
CHEMBL3905706 Ki = 1.5 nM 8.82
CHEMBL3939353 Ki = 1.7 nM 8.77
CHEMBL3965773 Ki = 2.0 nM 8.70
CHEMBL3932669 Ki = 2.1 nM 8.68
CHEMBL3948017 Ki = 2.1 nM 8.68
CHEMBL3933730 Ki = 2.1 nM 8.68
CHEMBL3907711 Ki = 2.1 nM 8.68
CHEMBL3945539 Ki = 2.3 nM 8.64
CHEMBL3907815 Ki = 2.3 nM 8.64
CHEMBL2105760 BREXPIPRAZOLE Ki = 2.3 nM 8.64
CHEMBL3956410 Ki = 2.5 nM 8.60
CHEMBL3969404 Ki = 2.6 nM 8.59
CHEMBL3957163 Ki = 2.6 nM 8.59
CHEMBL3902274 Ki = 2.8 nM 8.55
CHEMBL3929237 Ki = 2.8 nM 8.55
CHEMBL3905737 Ki = 2.9 nM 8.54
CHEMBL3903749 Ki = 2.9 nM 8.54
CHEMBL3902391 Ki = 2.9 nM 8.54
CHEMBL3976061 Ki = 3.0 nM 8.52
CHEMBL3901333 Ki = 3.0 nM 8.52
CHEMBL3905367 Ki = 3.1 nM 8.51
CHEMBL3907222 Ki = 3.1 nM 8.51
CHEMBL3977357 Ki = 3.2 nM 8.49
CHEMBL3893296 Ki = 3.3 nM 8.48
CHEMBL3980869 Ki = 3.3 nM 8.48
CHEMBL3985224 Ki = 3.3 nM 8.48
CHEMBL3961721 Ki = 3.4 nM 8.47
CHEMBL3966032 Ki = 4.0 nM 8.40
CHEMBL3931169 Ki = 4.0 nM 8.40
CHEMBL3953447 Ki = 4.1 nM 8.39
CHEMBL3892796 Ki = 4.2 nM 8.38
CHEMBL3893739 Ki = 4.3 nM 8.37
CHEMBL3916814 Ki = 4.4 nM 8.36
CHEMBL3935871 Ki = 4.5 nM 8.35
CHEMBL3944717 Ki = 4.6 nM 8.34
CHEMBL3974916 Ki = 4.9 nM 8.31
CHEMBL3909275 Ki = 5.0 nM 8.30
CHEMBL3944691 Ki = 5.1 nM 8.29
CHEMBL3953082 Ki = 5.3 nM 8.28
CHEMBL3912487 Ki = 5.5 nM 8.26
CHEMBL3907711 Ki = 5.7 nM 8.24
CHEMBL3958333 Ki = 5.7 nM 8.24
CHEMBL3899929 Ki = 6.1 nM 8.21
CHEMBL3941669 Ki = 6.3 nM 8.20